Faculty Publications
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Item An experimental investigation to determine the properties of fly ash based geopolymers as per indian standards(Springer, 2019) Saha, S.; C, C.Production of ordinary Portland cement requires huge quantity of natural resources and also releases huge quantity of carbon dioxide into the atmosphere. Research efforts have been continuing to establish geopolymer as an alternative cementitious material for the replacement of ordinary Portland cement. This paper presents the study to find out the properties of fly ash based geopolymer paste and 28 days compressive strength of geopolymer mortar. Standard consistency, setting time of geopolymer paste has been determined using vicat’s apparatus (according to Indian Standards), which is followed for cement paste, varying the concentration of sodium hydroxide solution from 6 to 16 M. Results indicate higher standard consistency, more time required for setting for fly ash based geopolymer than that of cement paste. Compressive strength of the geopolymer paste and mortar 17 specimens increases with the increase of the concentration of sodium hydroxide solution and decrease beyond 14 M. © 2019, Springer Nature Singapore Pte Ltd.Item Investigation on the potential use of recycled fine aggregate to produce geopolymer mortar mix(ASTM International, 2019) Saha, S.; C, C.The utilization of construction and demolition waste (C&DW) partially or fully for various purposes in construction industries is one of the most significant solutions to overcome the scarcity of raw materials and disturbances of the environmental system. On the other hand, geopolymer is being tried to be established as an alternative sustainable binder material for ordinary portland cement. In the present study, with the thought of promoting of sustainability, an attempt has been made to use concrete wastes as recycled fine aggregate (RFA) partially to produce fly ash (FA)-based geopolymer mortar. The workability, water absorption, compressive strength at 3, 7, 28, and 56 days, volume change behavior, and chloride permeability of the produced FA-based geopolymer mortar were determined. The effects of RFA, the ratio of alkali liquid (AL) to FA, and different curing regimes on these properties of mortar mix also discussed. The morphology and microstructures of the samples taken from the mortar mix, which were observed having the highest strength under different curing regimes, were studied using scanning electron microscopy (SEM). The experimental results indicate lower workability, higher water absorption capacity, and higher drying shrinkage of geopolymer mortar mix that has more RFA content in the mix, but the compressive strength of the geopolymer mortar mix started decreasing after a certain percentage of RFA content in the mix. Utilization of that certain percentage of RFA will help us to minimize the consumption of natural fine aggregates and reduce the disturbances generated by unorganized dumping of C&DW. © 2019 by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959.Item Characterization and performance of processed lateritic fine aggregates in cement mortars and concretes(Elsevier Ltd, 2019) Yaragal, S.C.; Basavana Gowda, S.N.; C, C.Availability of river sand is becoming scarce, due to rapid increase in infrastructure projects in India. Acute shortage of river sand, has led to indiscriminate sand mining. Adverse effect of sand mining includes river bank erosion, river bed degradation, loss of biodiversity and deterioration of river water quality and ground water availability. To address the above issues, research efforts are on, to find substitutes for river sand to be used as fine aggregate in mortars and concretes. One among the locally available resources is laterite. Laterite is a product of tropical or sub-tropical weathering, which is an abundant soil material in many parts of India. An attempt has been made to characterize the processing technique to obtain good quality lateritic fine aggregates (lateritic FA). Experiments were designed and conducted to study the performance of lateritic FA as replacement to river sand, in cement mortars and concretes. Processed lateritic FA in replacement levels of 0, 25, 50, 75 and 100 wt% to river sand at all fineness levels (Zone I to Zone IV as per Indian standards) is considered. Microstructure studies were conducted to understand the arrangement of river sand and lateritic FA with cement matrix and their Interfacial Transition Zones (ITZ) using Scanning Electron Microscope (SEM). The workability and compressive strength characteristics of cement mortars and concretes are evaluated. Laterized mortars with Zone III and Zone IV fine aggregates, at all replacement levels, result in the same compressive strengths as those of control mortars. Suitable strength enhancement technique has been attempted to achieve strengths of Zone I and Zone II lateritic fine aggregates based mortars at 100 wt% replacement, to achieve strength at least equal to or more than those of control mortars. Laterized concretes have achieved nearly the same strengths as those of control concretes, at all replacement levels and for all fineness levels (Zone I to Zone IV). © 2018 Elsevier LtdItem Volume change characteristics of eco-friendly mortar mixes produced with geopolymeric binder and recycled fine aggregate(ASTM International, 2020) Saha, S.; Shaik, N.; C, C.The production of geopolymer mortar using recycled fine aggregate (RFA) generated from concrete waste has significant potential to be a sustainable construction material. In this article, the volume change properties of the produced geopolymer mortar mixes are studied in terms of drying shrinkage up to the age of 180 days and reported as the percentage increase with respect to the shrinkage value of 3 days. The influence of RFA content, alkaline liquid (AL) in terms of the concentration of sodium hydroxide (SH) solution, the ratio of sodium silicate (SS) solution to SH solution, and the ratio of AL to fly ash (FA) were investigated on the drying shrinkage properties of the geopolymer mortar mixes. All the cast specimens were cured at 80°C for 24 hours. Higher drying shrinkage values were observed for the mortar mixes produced with higher RFA content, AL/FA, SS/SH ratio, and lower concentration of SH solution. Scanning electron microscope images were studied for the samples taken from the geopolymer mixes showing lower drying shrinkage values to understand the microstructure. © 2019 by ASTM International.Item Strength and shrinkage properties of heat-cured fly ash-based geopolymer mortars containing fine recycled concrete aggregate(ASTM International, 2020) Saha, S.; C, C.Geopolymer has obtained significant importance as an alternative eco-friendly binder material for ordinary portland cement (OPC) as it can be produced from the reaction between the industrial by-product materials rich in alumina, silica, and alkaline solutions. Therefore, usage of geopolymer effectively in the construction industry will help to reduce the consumption of a huge quantity of natural resources for the energy processes required for the production of OPC. It is also one of important solution to control carbon dioxides emission by the usage of OPC. On the other hand, using construction and demolition waste (C&DW) as the source of recycled aggregates in construction industry helps to reduce the huge consumption of natural aggregates and protect the environment from the disturbances caused by the unorganized dumping of C&DW. In this study, an attempt has been madeto produce fly ash (FA)-based geopolymer mortar mixes using C&DW effectively as fine aggregates partially. The effects of recycled fine aggregates (RFA), the ratio of alkaline liquid (AL) to FA, and duration of heat curing on the properties of the produced geo-polymer mortar mixes have been discussed in this article. To determine the influence of RFA on the strength and volume change behavior of mixes, natural fine aggregates were replaced by RFA at 0, 10, 20, 30, 40, and 50 % by mass. The AL/FA ratio was adopted as 0.4 and 0.6. Higher compressive strength was observed for most of the mortar mixes having RFA up to 20 %, and higher drying shrinkage value was found for the mixes with higher RFA content. Scanning electron microscopy (SEM) images were also studied for knowledge about the signature of the formed structures in the mortar mixes, which were observed having higher strength. © © 2019 by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959.Item Performance and microstructural investigations of processed lateritic fine aggregates in blended cement mortars exposed to elevated temperatures(Emerald Publishing, 2023) Basavana Gowda, S.N.; Yaragal, S.C.; C, C.; Goudar, S.K.Purpose: In recent years, fire accidents in engineering structures have often been reported worldwide, leading to a severe risk to life and property safety. The present study is carried out to evaluate the performance of Ground Granulated Blast Furnace Slag (GGBS) and fly ash–blended laterized mortars at elevated temperatures. Design/methodology/approach: This test program includes the replacement of natural river sand with lateritic fine aggregates (lateritic FA) in terms of 0, 50 and 100%. Also, the ordinary Portland cement (OPC) was replaced with fly ash and GGBS in terms of 10, 20, 30% and 20, 40 and 60%, respectively, for producing blended mortars. Findings: This paper presents results related to the determination of residual compressive strengths of lateritic fine aggregates-based cement mortars with part replacement of cement by fly ash and GGBS exposed to elevated temperatures. The effect of elevated temperatures on the physical and mechanical properties was evaluated with the help of microstructure studies and the quantification of hydration products. Originality/value: A sustainable cement mortar was produced by replacing natural river sand with lateritic fine aggregates. The thermal strength deterioration features were assessed by exposing the control specimens and lateritic fine aggregates-based cement mortars to elevated temperatures. Changes in the mechanical properties were evaluated through a quantitative microstructure study using scanning electron microscopy (SEM) images. The phase change of hydration products after exposure to elevated temperatures was qualitatively analyzed by greyscale thresholding of SEM images using Image J software. © 2023, Emerald Publishing Limited.Item Influence of the mix parameters on shrinkage properties of environment-friendly mortar(Taylor and Francis Ltd., 2024) Saha, S.; C, C.Cracks in concrete structures are generally initiated due to the shrinkage i.e. the volume change characteristics of the concrete structures. In this experimental study, effects of the mix parameters related to alkaline liquid (AL) and recycled fine aggregate (RFA) on the shrinkage behaviour of environment-friendly mortar mixes produced with fly ash (FA)-based geopolymer binder and RFA were investigated and reported. To find out the effects of AL, concentration of liquid sodium hydroxide (LSH) was varied from 6M to 16M, ratio of liquid sodium silicate (LSS) to LSH in AL was varied from 1.0 to 2.5 and AL/FA ratio was considered as 0.4 and 0.6. Different fly ash-based geopolymer mortar mix were produced depending on above-said combinations of mix parameters along with the RFA content (by weight) of 10%, 20%, 30%, 40% and 50% in lieu of natural fine aggregate. Prismatic specimens (25 mm × 25 mm × 285 mm) were cast and cured at ambient air temperature to determine the shrinkage behaviour. Higher RFA content in mix, higher LSS/LSH ratio in AL and higher AL/FA ratio resulted in higher shrinkage value. But, lesser shrinkage value was noticed for those specimens of mortar mix with the consideration of higher concentration of LSH in AL with varying RFA content. ©, Engineers Australia.