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    Flexural response of 3D printed sandwich composite
    (Elsevier Ltd, 2021) Bharath, H.S.; Bonthu, D.; Gururaja, S.; Prabhakar, P.; Doddamani, M.
    Among many lightweight materials used in marine applications, sandwich structures with syntactic foam core are promising because of lower water uptake in foam core amid face-sheets damage. HDPE (high-density polyethylene) filament is used to 3D print sandwich skin, and glass microballoon (GMB) reinforced HDPE syntactic foam filaments are used for the core. The optimized parameters are used to prepare blends of 20, 40, and 60 vol% of GMB in HDPE. These foamed blends are extruded in filament form to be subsequently used in commercially available fused filament fabrication (FFF) based 3D printers. The defect-free syntactic foam core sandwich composites are 3D printed all at once (skin-core-skin printing in sequence at once) using optimized printing parameters and characterized for the flexural behavior. The result reveals that the addition of GMB increases both specific modulus and strength in sandwich composites and is highest for the sandwich having a core with 60 vol% of GMB. The measured properties of sandwiches are compared with a respective core to study the effect of the sandwich. It is observed that flexural strength, fracture strength, and strain of foam core sandwiches registered superior response than their respective cores. The experimental results are found in good agreement with theoretical predictions. Finally, the failure mode of the printed sandwich is also discussed, and it is observed that none of the 3D printed syntactic foam core sandwiches fractured due to shear failure. © 2021 Elsevier Ltd
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    Additive Manufacturing of Short Silk Fiber Reinforced PETG Composites
    (Elsevier Ltd, 2022) Kn, V.; Bonthu, D.; Doddamani, M.; Pati, F.
    The growing demand for customized medical devices like prostheses, orthoses, and implants is the prime motive for a surge in the investigation of 3D printable biocomposites. PETG (Polyethylene terephthalate glycol) based composites can be a good choice for biomedical applications. Specific characteristics of this material like biocompatibility, ease of formability, stable thermomechanical properties, and high chemical, and abrasion resistance make it suitable for biomedical applications. However, there are very few studies on the 3D printing of PETG-based composites. Development of a robust 3D printing protocol is required for any novel natural fiber reinforced PETG composites. This study presents natural fiber-reinforced PETG biocomposite filament preparation and 3D printing with the developed composite filaments. Silk was used as a filler material due to its high thermal stability and high tensile strength. Composite filaments with 2 wt%, 5 wt%, and 10 wt% silk were prepared using the extrusion process. Further, we developed a protocol for 3D printing with the developed composites to fabricate various 3D structure. Both filaments and printed specimens were characterized morphologically, structurally, and mechanically. The melt flow rate of the filaments decreased with an increase in fiber content which was a bottleneck for printing 10% silk-PETG composites. Micro-CT results validate an increase in void content in filaments on filler addition. The highest flexural modulus and flexural strength were exhibited by 2% silk-PETG printed parts and a 60% increase in compressive modulus compared to pure PETG. Tensile tests show that 2 wt% fiber addition significantly increased elastic modulus (2466.72 MPa) compared to pure PETG (902.81 MPa), whereas the surface roughness of printed composites increased with filler content. Finally, a lower limb prosthetic socket prototype was printed with a desktop 3D printer to demonstrate its potential for biomedical applications. © 2022 Elsevier Ltd