Faculty Publications
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Item Influence of Process Parameters on Microstructural Properties of L-DED Produced Ti64 Alloy(Springer Science and Business Media Deutschland GmbH, 2025) Suresh, S.; Kuriachen, B.; Kumar, V.; Bontha, S.; Gurugubelli, R.C.Additive manufacturing (AM) techniques have revolutionized the manufacturing of complex and customized parts across various applications. However, they are known for producing titanium parts with high anisotropy and low ductility, due to high cooling gradient in the build direction and the presence of martensite phase in microstructure respectively. These are inherent problems which limit their application in critical engineering fields. Laser—Direct Energy Deposition (L-DED) produced parts also have the same disadvantages. Thus, the primary objective of this paper is to identify the optimal combination of process parameters for L-DED that can mitigate these inherent limitations. Keeping the parameters such as powder size, orientation angle and hatch angle as constant, the laser power and scan speed are varied to fabricate 9 different sets of samples using L-DED. The research methodology includes an analysis of the microstructure, focusing on grain width, phase distribution, lath characteristics and presence of defects, if any. Microscopy and XRD techniques were used to observe the microstructure. Additionally, hardness studies were performed to evaluate the changes in material hardness. It was noticed that laser power significantly influences β width and α’ length while scan speed has a lesser dominant effect on both of them. The findings will contribute to the development of process-structure-property relations for L-DED-produced Ti64 and further, optimized manufacturing strategies for producing titanium parts with reduced anisotropy and increased ductility. © The Author(s), under exclusive license to Springer Nature Singapore Pte Ltd. 2025.Item Effect of heat treatment on microstructure, corrosion, and shape memory characteristics of laser deposited NiTi alloy(Elsevier Ltd, 2018) Marattukalam, J.J.; Balla, V.K.; Das, M.; Bontha, S.; Kalpathy, S.K.The aim of this work is to study the effect of heat treatment on the microstructure, phase transformations, shape memory characteristics and corrosion behaviour of laser deposited equiatomic NiTi alloy. Dense samples of NiTi alloy were fabricated using Laser Engineered Net Shaping (LENS™) with two different laser energy densities by varying the scan speed and laser power. These samples were annealed for 30 min at 500 °C and 1000 °C in flowing argon, followed by furnace-cooling to room temperature. The resulting microstructures and properties were compared with the corresponding as-deposited samples. Microstructural analysis after heat treatment showed needle-shape martensite in the samples processed at lower laser energy density of 20 J/mm2, and lenticular or plate-like martensite in the samples processed at 80 J/mm2. The XRD results revealed relatively high concentration of martensite (B19?) in heat-treated NiTi alloy compared to as-processed samples. Furthermore, the heat treatment decreased the forward and reverse transformation temperatures of NiTi alloy from 80 – 95 °C to 20–40 °C, presumably due to annihilation of thermally induced defects. Interestingly, the samples annealed at 500 °C showed a measurable increase of 1–2% in the shape memory recovery, from the net recovery of 8% exhibited by the as-processed NiTi alloy. The corrosion resistance of laser-processed NiTi alloy decreased upon annealing. © 2018 Elsevier B.V.Item Microstructure, mechanical and wear properties of the A357 composites reinforced with dual sized SiC particles(Elsevier Ltd, 2019) Avinash, A.; Bontha, S.; Krishna, M.; Koppad, P.G.; Ramprabhu, T.Current work reports on the development of A357 alloy composite which is reinforced with dual size SiC particles by stir casting route. Influence of different weight fractions (3% coarse+ 3% fine, 4% coarse + 2% fine, and 2% coarse + 4% fine) of dual size SiC particles on mechanical properties and wear resistance of A357 composites is the focus of this work. Hardness and tensile properties were studied for dual size composites and then were compared with A357 alloy. Microstructural study, fractured surface and worn surface investigation were carried out using optical and scanning electron microscopes respectively. Microstructural analysis showed fairly uniform dispersion of dual size SiC particles in A357 matrix with good interfacial bonding. Compared to A357 alloy, the composites showed improvement in hardness, yield, and tensile strength. In particular, composite with 4 wt. % of fine and 2 wt. % of large SiC particles displayed the highest tensile strength while composite with 4 wt. % of large and 2 wt. % of fine SiC particles exhibited high hardness and wear resistance among A357 alloy and dual particle size composites. The strengthening mechanisms that contributed to improvement in strength values were effective load transfer and dislocation strengthening due to thermal mismatch. © 2019 Elsevier B.V.
