Faculty Publications
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Item Comparative investigation of coating and friction stir processing on Mg-Zn-Dy alloy for improving antibacterial, bioactive and corrosion behaviour(Elsevier B.V., 2021) Rokkala, U.; Jana, A.; Bontha, S.; Ramesh, M.R.; Balla, V.K.Magnesium based alloys are well-known materials for temporary implant applications. However, failures due to early degradation and bacterial infection are limiting their applications. To overcome these problems, in the present work a Mg-Zn-Dy alloy based composite surface was prepared using coating and friction stir processing (FSP) techniques. Herein, hydroxyapatite (HA) and silver (Ag) particles were deposited on Mg-Zn-Dy alloy to obtain HA and Ag coated surface (C-HAg). Later, FSP was carried out on the C-HAg surface to develop a Mg-Zn-Dy alloy based composite surface (F-HAg). Field emission scanning electron microscope (FESEM) and energy dispersive X-ray analysis (EDS) confirm the mixing of HA and Ag particles with the Mg-Zn-Dy substrate. Antibacterial studies reveal that both C-HAg and F-HAg samples inhibit Escherichia coli and Staphylococcus aureus bacteria. In vitro cytotoxicity study indicates that the both samples are non-toxic in nature. Results of in vitro corrosion study reveal a significant reduction (72%) in corrosion rate of F-HAg sample when compared to C-HAg sample. The F-HAg samples showed simultaneous improvement in corrosion resistance and antibacterial properties with good biocompatibility. The results of this study indicate that the developed composite surface is a promising material for antibacterial and biodegradable implant applications. © 2021 Elsevier B.V.Item Influence of friction stir processing on microstructure, mechanical properties and corrosion behaviour of Mg-Zn-Dy alloy(Springer, 2023) Rokkala, U.; Bontha, S.; Ramesh, M.R.; Balla, V.K.In the present study, friction stir processing (FSP) was carried out on as-cast Mg-Zn-Dy alloy to tailor grain size and texture which alter the mechanical properties and corrosion behaviour. The grain size of the as-cast alloy was reduced from 60 ± 2 µm to 3 ± 0.1 µm after FSP due to dynamic recrystallization. The effect of grain size, crystallographic orientation and fine precipitates on mechanical properties were investigated using field emission scanning electron microscope (FESEM) and electron back scattered diffraction (EBSD). The ultimate tensile strength, yield strength, % elongation and hardness of FSPed alloy improved by 55%, 60%, 53% and 46% when compared to as-cast alloy. The FSPed Mg-Zn-Dy alloy exhibited a 79% decrease in corrosion rate when compared to as-cast alloy which can be attributed to grain refinement, uniform distribution of secondary precipitates and strong basal texture. The surface of FSPed sample after immersion corrosion exhibited calcium phosphate rich minerals which help in apatite formation on the sample surface. Cytotoxicity studies using MTT assay revealed more than 80% cell viability for both as-cast and FSPed alloy illustrating non-toxic nature of both the samples. The results of this study indicate that FSPed Mg-Zn-Dy alloy is a potential material for biodegradable implants due to its high strength, corrosion resistance and biocompatibility. Graphical Abstract: [Figure not available: see fulltext.]. © 2023, The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature.Item Effect of equiaxed grains and secondary phase particles on mechanical properties and corrosion behaviour of CMT- based wire arc additive manufactured AZ31 Mg alloy(Elsevier Ltd, 2023) Manjhi, S.K.; Sekar, P.; Bontha, S.; Balan, A.S.S.Wire arc additive manufacturing (WAAM) has drawn tremendous attention for manufacturing large and complex components of lightweight material at a moderate cost due to its high deposition rate and energy efficiency. Generally, WAAM-Mg alloy comprises columnar and columnar dendrite grains due to high cooling rates and thermal gradients responsible for anisotropic mechanical properties. To overcome this challenge, in this work, CMT-WAAM, which generally uses comparatively low heat input (33% lower than conventional WAAM), was used to deposit AZ31 Mg thin wall. The metallurgical characterization of the deposited thin wall of the top (T), middle (M) and bottom (B) sections reveals equiaxed grains of average sizes ∼ 58, ∼ 63 and ∼ 38 µm, respectively. In addition, TEM results exhibit the formation of secondary phase particles, i.e., β-Mg17Al12 and ɳ-Al8Mn5. Further, the ultimate tensile strength (UTS) and % elongation (% EL) in the travel direction (UTS = 224 MPa, % EL= 23.47%) are superior to that obtained in the build direction (UTS = 217 MPa, % EL = 20.82%). The corrosion resistance of WAAMed AZ31 Mg alloy is higher than wrought (cold rolled) AZ31 Mg alloy in Hank's balanced salt solution (HBSS). The results of this study reveal the potential of CMT-WAAM to deposit different grades of Mg with desired microstructure, mechanical properties and corrosion resistance. © 2023 CIRPItem Unveiling the role of heat treatment approaches in tailoring corrosion performance of laser powder-directed energy deposited SS304(Elsevier B.V., 2025) Sasindran, J.; Narayanan, J.A.; Babu, I.A.; Balan, A.S.S.; Hebbar, H.S.; Bontha, S.This study investigates the effect of different post-processing heat treatment approaches on the corrosion behavior of Laser Powder-Directed Energy Deposited (LP-DED) SS304. Samples were fabricated using optimized LP-DED parameters: laser power of 400 W, scan speed of 800 mm/min, feed rate of 4 g/min, 0.6 mm beam diameter, and 33 % track overlap.Electrochemical analysis revealed significant differences in corrosion performance depending on the applied heat treatment approach. This treatment resulted in changes to residual stress, microstructure, and oxide layer characteristics which together influence the corrosion rate (CR). The stress-relief annealed (SRA) samples significantly improved corrosion resistance by up to 90 % compared to the as-built condition, while preserving the fine microstructure formed during the LP-DED process and maintaining a stable protective oxide layer. Solution treated and different quenched samples exhibited varying CR depending on the cooling rate and resulting coarse grain structure. These findings highlight the significant influence of post-processing heat treatments on corrosion behavior and microstructural characteristics. © 2025 Elsevier B.V.