Faculty Publications
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Item Effect of Cryogenics-Assisted Low-Plasticity Burnishing on Laser-Clad Stellite 6 over SS420 Substrate(Springer, 2020) Anirudh, P.V.; Kumar, B.; Girish, G.; Shailesh, S.; Oyyaravelu, R.; Kannan, C.; Balan, A.S.S.The influence of modern additive manufacturing methods, especially from the direct energy deposition (DED) processes to the coat-like finished components, is crucial under present industrial circumstances. DED induces several traits like enhanced mechanical, thermal properties in shorter lead time, which extend their adaptation for diverse applications including aerospace and automobile industries. Among the several DED processes, laser cladding has been a prospect that explores various capabilities of improving the wear resistance of cobalt-chromium (Co-Cr)-based alloys. Rather than fabricating the complete component using expensive alloys, laser cladding has paved an approach to deposit particles possessing superior qualities over the conventional material. This research work attempts to evaluate the surface integrity of SS420 when cladded with Stellite 6. The vertical face milling is executed on the cladded component surface to facilitate either low-plasticity burnishing (LPB) or cryogenic burnishing (CB) as sequential post-treatment processes. The effects of these post-treatments on the surface and subsurface microhardness, surface topography and residual stress profiles are elaborated. Increased surface and subsurface microhardness, as well as improved residual stress profiles, are observed with CB over LPB-processed specimen samples. © 2020, ASM International.Item Hybrid additive manufacturing of ER70S6 steel and Inconel 625: A study on microstructure and mechanical properties(Elsevier Ltd, 2023) Rodrigues, J.P.; Thanumoorthy, R.S.; Manjhi, S.K.; Sekar, P.; Arumuga Perumal, D.A.; Bontha, S.; Balan, A.S.S.Hybrid Additive Manufacturing (HAM) is currently being explored because of its potential to achieve trade-off between build capacity and feature resolution. The present study aims at fabricating ER70S6-Inconel 625 (IN625) bimetallic clad using hybrid Wire Arc Additive Manufacturing (WAAM) and Laser Directed Energy Deposition (LDED) processes. Microstructure evaluation was performed at the cross section of bimetallic clad for distinct materials as well as the interface. WAAM built ER70S6 revealed equiaxed ferritic grains, whereas laser deposited IN625 region showed columnar dendrites with under developed secondary arms. However, the first layer of IN625 exhibited columnar dendrite with secondary arms due to the influence of diffused Fe from the base ER70S6 steel under the action of concentrated laser heat source, which was revealed by energy dispersive spectroscopy (EDS) maps. The measured microhardness across the cross section of the deposit showed values corresponding to inherent material system. The interface did not reveal presence of any intermetallic phases which was confirmed by hardness results and X-Ray diffraction. Shear test revealed superior bond strength between the two materials, maintaining average strength of 452 MPa. The fractography images exhibited fine dimples along with cleavages indicating mixed fracture characteristics. This additive manufacturing method explores a new dimension in multi-material fabrication which, when customized for different materials, serve critical areas in the aerospace and defence sector. © 2023 Elsevier LtdItem Surface Characteristics of Low Plasticity Burnished Laser Directed Energy Deposition Alloy IN718(Springer, 2024) Mohanraj; Thanumoorthy, R.S.; Sekar, P.; Muthuchamy, A.; Bontha, S.; Balan, A.S.S.The research work focuses on a novel post-processing sequence to improve the surface integrity and residual stress characteristics of as-printed Inconel718 (IN718) samples. The as-printed IN718 samples are subjected to solution treatment at 1050 °C, two-step precipitation hardening (@ 720 °C for 8 h and @ 620 °C for 8 h), and low plasticity burnishing. Two different sequences were attempted. Sequence-1 involves solutionizing ? low plasticity burnishing followed by precipitation hardening, and sequence-2 includes solutionizing ? precipitation hardening followed by low plasticity burnishing. The experimental observations and detailed investigations revealed that the samples processed via sequence 2 exhibited a better surface finish. The microhardness of the samples of sequence 2 is 10% higher than their counterparts in sequence 1. The maximum residual stress of ?1375.33 MPa is obtained in sequence 1 as compared to the residual stress of ?1100.67 MPa in sequence 2. The influence of the processing sequences on the surface properties has been discussed in detail using the XRD and microstructural characterization supported with EBSD analysis. Graphic Abstract: (Figure presented.) © The Indian Institute of Metals - IIM 2024.Item Effect of age hardening precipitates on the corrosion performance of laser Powder-Directed energy deposited CuNi2SiCr(Elsevier B.V., 2024) Urs, S.S.; Thanumoorthy, R.S.; Aswith Babu, I.; Doddamani, M.; Bontha, S.; Balan, A.S.S.This study explores Laser Powder ? Direct Energy Deposition (LP-DED) processing of CuNi2SiCr and the effect of heat treatment on corrosion behavior. The findings pave the way to increasing the life of the components and the possibility of refabrication upon failure. LP-DED manufactured CuNi2SiCr was subjected to solution treatment followed by age-hardening at 500? for 1,3,5 and 7 h. The microstructure analysis showed the formation of Cr3Ni precipitates due to a higher cooling rate in the LP-DED process. Upon aging, Ni3Si, Ni2Si, and CrSi2 precipitates evolved. Due to the Orowan phenomenon, microhardness increases with the aging time as the number of precipitates along the grain boundary increases with the aging time. The 5-hour aged sample exhibited the best corrosion resistance due to precipitation coherency in the matrix and the medium-sized precipitates with uniform precipitation-free zones (PFZ) in the grain boundary. © 2024 Elsevier B.V.Item A novel NiCrAlY-Cu based bond coat for rocket nozzle applications through LP-DED process(Elsevier Ltd, 2025) Thanumoorthy, R.S.; Vijay, A.; Bontha, S.; Balan, A.S.S.This study explores the development of a novel bond coat for copper-based substrates with the goal of minimizing thermal expansion mismatch and enhancing thermal life in rocket nozzle applications. The effect of copper (Cu) addition on the microstructure, phase evolution, and thermo-mechanical behavior of NiCrAlY clads fabricated via laser powder-directed energy deposition (LP-DED) is systematically investigated to optimize their performance. SEM and elemental mapping reveal a shift from columnar to cellular substructures with Cu additions up to 20 wt%, while higher Cu contents lead to coarse dendritic growth and Cu segregation at grain boundaries, inducing localized strain and crack formation. XRD and DFT analyses indicate that Cu suppresses the ?-NiAl phase and stabilizes the ?-Ni matrix due to its limited solubility in ? and preferential partitioning into ?. High-temperature XRD and EDS analyses show that while pure NiCrAlY forms a continuous alumina scale, Cu-enriched clads develop fragmented and crack-prone thermally grown oxides (TGOs), compromising the oxidation resistance. KAM analysis suggests reduced lattice strain at 10 wt% Cu, followed by increased dislocation density at higher concentrations. Thermal expansion measurements indicate a significant increase in the coefficient of thermal expansion (CTE) at 10 wt% Cu, improving compatibility with Cu-based substrates. However, further Cu additions yield minimal CTE benefits while degrading mechanical strength. Microhardness declines from ?406 Hv (0 % Cu) to ?251 Hv (40 % Cu) due to solid solution softening and ?-phase suppression. A radar plot comparing key metrics identifies 10 wt% Cu as the optimal composition, offering a balanced property set for regeneratively cooled rocket nozzle systems. © 2025 Elsevier B.V.
