Faculty Publications
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Item Microstructure Evolution and Mechanical and Corrosion Behavior of Accumulative Roll Bonded Mg-2%Zn/Al-7075 Multilayered Composite(Springer New York LLC barbara.b.bertram@gsk.com, 2017) Anne, G.; Ramesh, M.R.; Shivananda Nayaka, H.; Arya, S.B.; Sahu, S.Multilayered composite of Mg-2%Zn/Al-7075 was developed by accumulative roll bonding (ARB) of wrought Mg-2%Zn and aluminum 7075 alloy. The Mg-2%Zn/Al-7075 multilayered composite exhibited density of 2295 kg/m3 and an average grain size of 1 and 1.3 ?m in Mg-2%Zn and Al-7075 layers, respectively. A thorough microstructural characterization was performed on the composites by scanning electron microscope, electron backscatter diffraction (EBSD), transmission electron microscope and phase analysis by x-ray diffraction. In addition, mechanical properties were evaluated by microhardness and tensile tests. Corrosion behavior of the multilayered composite was examined using electrochemical polarization test. EBSD analysis showed the presence of ultrafine grains with high-angle grain boundaries. The composite exhibited a significant improvement in ultimate tensile strength (~1.82 times) and elongation (~1.5 times) as compared with Mg-2%Zn alloy, after four-pass ARB process. © 2017, ASM International.Item Development and properties evaluation of Mg-6% Zn/Al multilayered composites processed by accumulative roll bonding(Cambridge University Press, 2017) Anne, G.; Ramesh, M.R.; Shivananda Nayaka, H.; Arya, S.B.; Sahu, S.Accumulative roll bonding (ARB) process was used to develop Mg-6% Zn/Al and Mg-6% Zn/anodized-Al multilayered composites. Microstructural characterization was done using scanning electron microscopy, energy-dispersive X-ray spectroscopy, electron backscattered diffraction, and transmission electron microscopy. An average grain size measured in the roll-bonded layers of Al, anodized Al, and Mg-2% Zn was found to be 1.8 ?m, 1.6 ?m, and 0.6 ?m, respectively. Phases Al17Mg12, AlMg4Zn11, and Al2O3 after 5-pass of ARB were confirmed by X-ray diffraction analysis. The Mg-6% Zn/Al and Mg-6% Zn/anodized Al composites exhibited tensile strengths ?252 MPa and ?256 MPa, respectively, after a 5-pass ARB process. Hardness of the individual layers of composite increased linearly with an increase in the number of ARB passes. Fractographs of the multilayered composite illustrated the ductile failure in Al and anodized Al layers and transgranular brittle fracture in Mg-6% Zn layers. © Materials Research Society 2017.Item Effects of combined multiaxial forging and rolling process on microstructure, mechanical properties and corrosion behavior of a Cu-Ti alloys(Institute of Physics Publishing helen.craven@iop.org, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.; Sahu, S.; Arya, S.Combined multiaxial forging (MAF) and rolling was performed on Cu-3% Ti (wt%) alloy at room temperature with emphasis on microstructural evolution, improvement in mechanical properties, and corrosion resistance. Microstructural changes were confirmed from various characterization techniques, and co-related with mechanical properties. TEM analysis revealed high shear band density in the 3 pass MAF + 90% rolled sample appearing due to high strain. EBSD analysis revealed transformation to low angle grain boundaries from high angle grain boundaries. Maximum microhardness and UTS reached to 340 HV and 960 MPa, respectively in the processed samples. Significant grain refinement was observed in MAF processed Cu-3%Ti alloy, and after combined MAF + rolling, higher dislocation density and refinement of shear bands were observed. In addition, potentio-dynamic polarization test was used to study the corrosion behavior of the alloy. Scanning electron microscope (SEM) was used to analyze the corroded surface morphology. © 2019 IOP Publishing Ltd.Item Influence of Multidirectional Forging on Microstructural, Mechanical, and Corrosion Behavior of Mg-Zn Alloy(Springer New York LLC barbara.b.bertram@gsk.com, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.S.; Sahu, S.; Ramesh, M.R.Multidirectional forging (MDF) was applied to Mg-6%Zn alloy up to 5 passes successfully at 280 °C. MDF-processed materials were characterized using optical microscope, scanning electron microscope, electron backscatter diffraction, transmission electron microscope, and x-ray diffraction. Obtained results showed a significant reduction in grain size (up to 3.8 ?m) having a large fraction of high-angle grain boundaries after 5 passes of MDF process. Maximum tensile strength of 230 MPa was achieved for 5-pass MDF-processed Mg-6%Zn alloy which is about ~ 2.0 times higher in comparison with that of homogenized alloy (117 MPa) and was attributed to higher dislocations density and grain refinement. Corrosion behavior of the alloy was investigated in 0.1 M NaCl solution using potentiodynamic polarization test, electrochemical impedance spectra analysis, and immersion tests. It was found that the corrosion rate of 5-pass MDF sample improved (0.34 mm/year) ~2.5 times in comparison with that of homogenized Mg-6%Zn alloy (0.86 mm/year) due to fine grain structure, which creates more grain boundaries that act as a corrosion barrier. © 2019, ASM International.Item Investigation of dry sliding wear properties of multi-directional forged Mg–Zn alloys(National Engg. Reaserch Center for Magnesium Alloys zhangdingfei@cqu.edu.cn, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.S.; Sahu, S.; Ramesh, M.R.Effect of multi-directional forging (MDF) on wear properties of Mg–Zn alloys (with 2, 4, and 6 wt% Zn) is investigated. Dry sliding wear test was performed using pin on disk machine on MDF processed and homogenized samples. Wear behavior of samples was analyzed at loads of 10 N and 20 N, with sliding distances of 2000 m and 4000 m, at a sliding velocity of 3 m/s. Microstructures of worn samples were observed under scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and x-ray diffraction (XRD) and the results were analyzed. Mechanical properties were evaluated using microhardness test. After 5 passes of MDF, the average grain size was found to be 30 ± 4 µm, 22 ± 3 µm, and 18 ± 3 µm, in Mg–2%Zn, Mg–4%Zn, and Mg–6%Zn alloys, respectively, with significant improvement in hardness in all cases. Wear resistance was improved after MDF processing, as well as, with increment in Zn content in Mg alloy. However, it decreased when the load and the sliding distance increased. Worn surface exhibited ploughing, delamination, plastic deformation, and wear debris along sliding direction, and abrasive wear was found to be the main mechanism. © 2019Item Influence of Ball Burnishing Process on Equal Channel Angular Pressed Mg-Zn-Si Alloy on the Evolution of Microstructure and Corrosion Properties(Springer Science and Business Media B.V., 2021) Ramesh, S.; Anne, G.; Kumar, G.; Jagadeesh, C.; Shivananda Nayaka, H.In the present study, Mg-4Zn-1Si alloy was subjected to equal channel angular pressing (ECAP) up to 4 passes at 300 °C, followed by ball burnishing using 0.3 mm depth of press, 300 mm/min feed and 1 pass successfully. The effect of ECAP and ECAP + ball burnishing process on microstructure, mechanical properties (tensile and hardness) and corrosion behavior was systematically investigated. After 4 pass ECAP, initial coarse grains (210 ?m) were refined and average grain size is 6 ?m and after ball burnishing, the grain size is found to be 3.3 ?m. Microstructure evolution is discussed using optical images, scanning electron microscope images and transmission electron microscope images. For ECAP samples, maximum strength and hardness was recorded at 3 pass. Both strength and hardness decreased for 4 pass ECAP processed samples, even though grain size decreased, this is because of texture modification in the material. ECAP 4 pass + ball burnished samples exhibited 48.5% enhancement of microhardness as compared to 4 pass ECAP samples. Corrosion resistance of the samples decreased with increase in the number of ECAP passes, this is due to strain-induced grain refinement with more crystalline defects in samples. Combined process of ECAP and ball burnishing effectively reduces the Icorr and this consequently reduces corrosion rate of the Mg–4Zn-1Si alloy. © 2020, Springer Nature B.V.Item Solid Particle Erosion Behaviour of Plasma-Sprayed (WC–Co)/(Cr3C2–NiCr) Coatings(Springer Science and Business Media Deutschland GmbH, 2022) Reddy, G.M.S.; Ramesh, S.; Anne, G.; Ramesh, M.R.; Rao, T.N.; Patil, P.This study reports the high-temperature erosion behaviour of plasma-sprayed 35% (WC–Co)/65% (Cr3C2–NiCr) coating on MDN-420 alloy. Plasma spray coatings have always played a pivotal role in enabling industries to combat problems of premature degradation of components that operate in harsh environments. (WC–Co) + (Cr3C2–NiCr) coating is investigated for erosion under various laboratory-simulated conditions. Coating surface is characterized by using an optical microscope, scanning electron microscope (SEM), and X-ray diffraction (XRD). Porosity, microhardness, surface roughness, and adhesion strength of the coating are measured. The solid particle erosion test is conducted at the temperatures of 300 °C, 500 °C and 700 °C with the impact angles of 30° and 90° by using Al2O3 as an erodent in the hot air jet erosion testing machine. The optical profilometer is used to evaluate the erosion volume loss of the coated and uncoated samples. It is observed that erosion resistance of the substrate is found to be higher than the coating at the different test temperatures. As the temperature increases, the erosion resistance of the coating is also increased at all the temperatures for both impact angles of 30° and 90°.The eroded coating surface morphology reveals that the generalized behaviour of the coating is ductile in nature. © 2022, The Author(s), under exclusive licence to Springer Nature Switzerland AG.Item Investigation of Tribological Characteristics of Cu-Ti Alloys Processed by Multi-Axial Cryo-Forging(Springer, 2022) Ramesh, S.; Shivananda Nayaka, H.S.; Anne, G.; Arun, M.N.; Naik, G.M.Cu-XTi alloys (X = 1.5 and 4.5%) were subjected to multi-axial forging (MAF) under cryogenic condition up to three passes successfully. Characteristics of the MAF-processed alloys were analyzed using microstructural analysis, hardness and wear tests. Worn surface morphology and elemental analysis was performed by scanning electron microscopy. The hardness of samples increases with higher MAF passes due to strain hardening and grain refinement. Wear test was done for six various sliding distances (500, 1000, 1500, 2000, 2500 and 3000 m), two different loads (10 and 20 N), and two different velocities (1 and 2 m/s) using the pin-on-disk wear test rig. Wear loss of as-received samples is higher than MAF-pressed samples due to an increase in hardness, but wear loss increases as the load increases. Coefficient of friction is reduced with the increase in MAF pass, which is due to strain hardening effect. The worn surface exhibits the plastic deformation regions, delamination, plowing and formation of oxide layers, which was revealed by energy-dispersive X-ray spectroscopy analysis. Also, MAF-processed samples exhibited abrasive wear mechanism as a result of formation of oxygen layer as revealed in SEM micrographs. © 2022, ASM International.Item Enhancing surface characteristics of Mg-Zn-Sr alloy through cryo-ball burnishing; modeling and experimentation(Korean Society of Mechanical Engineers, 2024) Kudva, S.A.; Anne, G.; Ramesh, S.; Sharma, P.; Jagadeesh, C.; Ritti, L.; Naik, G.M.; Divya Deepak, G.D.In this investigation, the impact of the cryo-ball burnishing process on both the mechanical and corrosion properties of the Mg-4Zn-1Sr alloy was systematically explored. To better understand the plastic deformation occurring in Mg-4Zn-1Sr during cryo-burnishing, a finite element analysis (FEA) model was developed. The microstructure of cryo-ball burnished samples underwent characterization through scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffractometry (XRD), and surface properties were assessed using atomic force microscopy (AFM). Additionally, electrochemical impedance spectroscopy and potentiodynamic polarization tests were conducted in a simulated body fluid using an electrochemical workstation. Experimental findings revealed significant grain refinement and the presence of residual dislocations during the cryo-burnishing process, as evident in TEM analysis. XRD analysis indicated the presence of Mg, Mg17Sr2 and SrZn2 phases, with observable peak broadening in the cryo-burnished samples, attributed to structural refinement and lattice strain incorporation. Microhardness values increased with greater depth of press, with the DFN 1071 sample displaying a hardness of 80 ± 4 Hv (Ra = 1.853 µm), marking a 54 % improvement compared to the homogenized sample. The enhanced corrosion resistance of the Mg-4Zn-1Sr alloy due to cryo-burnishing is attributed to the combined effects of grain refinement, residual dislocations, and intermetallic phases. © The Korean Society of Mechanical Engineers and Springer-Verlag GmbH Germany, part of Springer Nature 2024.Item Impact of ply stacking sequence on the mechanical response of hybrid Jute-Banana fiber phenoplast composites(Institute of Physics, 2024) Maruthi Prashanth, B.H.; Ramesh, S.; Shivakumar Gouda, P.S.S.; Naik, G.M.; Sharma, P.; Jagadeesh, C.; Mahantesh, M.M.; Anne, G.Natural fiber composites are increasingly gaining popularity as a cost-effective and environmentally friendly alternative to synthetic fibers. Incorporating a variety of fibers enhances mechanical properties. The arrangement of fibers plays a crucial role in determining the mechanical characteristics of laminate composites. Therefore, the primary objective of this study is to investigate how the stacking order of jute (J) and banana (B) fibers affects the mechanical behaviour of composites made from phenolic resins. Four different fiber mat stacking sequences (J/B/B/J, B/J/J/B, J/B/J/B, and J/J/B/B) were used for developing the eco-fiber composites using the heat-press technique. Several mechanical parameters were assessed, including tensile strength, flexural strength, impact strength, and inter-laminar shear strength (ILSS). The experimental results indicated that the JBBJ composite exhibits superior tensile strength (46.65 MPa) and modulus (993 MPa) compared to the other composites due to the presence of high-strength jute fibers on the surface. Additionally, the flexural strength of the JBBJ composite (87.24 MPa) was found to be noteworthy. It was observed that the impact strength of jute fibers surpasses that of banana fibers. Consequently, the JBBJ composite demonstrates higher values for energy absorption (0.482 J) and impact strength (120 J m−1) compared to the other composites tested. Moreover, the JBBJ composite displays higher inter-laminar shear strength and hardness values compared to BJJB, JBJB, and JJBB by 30%, 35%, and 43%, respectively. Scanning electron microscope microphotographs reveal strong correlational fracture failure mechanisms, indicative of improved mechanical properties in the JBBJ composite. Based on the experimental results, it is evident that the JBBJ composite can be utilized in lightweight applications. © 2024 The Author(s). Published by IOP Publishing Ltd.