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Item Cu-44Ni-5Cr alloy has been subjected to thermomechanical treatment which consisted of plastic deformation of as-quenched material by 50, 65 and 80% reduction in thickness followed by ageing in the interval of 500 to 650 °C for various durations of time. Progress in age-hardening was studied by means of hardness measurement and X-ray diffraction studies. The wavelength of composition modulation and strain amplitude were measured. It was found that age-hardening was a result of interaction between spinodal decomposition and recovery processes. Prior deformation was found to enhance the kinetics of both spinodal decomposition and coarsening. It was concluded that this resulted from increased vacancy concentration and increased coherency strain in the cold-worked material. © 1994 Chapman & Hall.(Kluwer Academic Publishers, Effect of thermomechanical treatment on the phase transformation in Cu-44Ni-5Cr alloy) Raghavendra Bhat, R.; Prasad Rao, P.1994Item Progress in spinodal decomposition of a Cu-32Ni-2Cr alloy subjected to quench?age and quench?work?age treatments have been studied through hardness measurements as well as by X-ray diffraction techniques. It is found that recovery processes occur during early stages of aging which are interpreted in terms of the migration of matrix dislocations to interfaces. The kinetics of spinodal decomposition is found to be enhanced by prior deformation. Thermomechanical treatment results in a substantial increase in strength.(Publ by Carl Hanser Verlag GmbH & Co, Thermomechanical treatment of spinodal Cu-32Ni-2Cr alloy) Bhat, R.Raghavendra; Prasad Rao, P.1994Item [No abstract available](Springer Netherlands, Low cycle fatigue behavior of an (? + ?) titanium alloy) Nanjundaswamy, G.S.; Ramachandra, C.; Sengupta, P.K.; Chatterji, B.; Sudhakara Nayak, H.V.; Singh, A.K.1998Item Heat transfer during quenching of modified and unmodified gravity die-cast A357 cylindrical bars(2006) Prabhu, K.; Hemanna, P.Heat transfer during quenching of chill-cast modified and unmodified A357 Al-Si alloy was examined using a computer-aided cooling curve analysis. Water at 60°C and a vegetable oil (palm oil) were used as quench media. The measured temperatures inside cylindrical probes of the A357 alloy were used as inputs in an inverse heat-conduction model to estimate heat flux transients at the probe/quenchant interface and the surface temperature of the probe in contact with the quench medium. It was observed that modified alloy probes yielded higher cooling rates and heat flux transients. The investigation clearly showed that the heat transfer during quenching depends on the casting history. The increase in the cooling rate and peak heat flux was attributed to the increase in the thermal conductivity of the material on modification melt treatment owing to the change in silicon morphology. Fine and fibrous silicon particles in modified A357 probes increase the conductance of the probe resulting in higher heat transfer rates. This was confirmed by measuring the electrical conductivity of modified samples, which were found to be higher than those of unmodified samples. The ultrasound velocity in the probes decreased on modification. ©ASM International.Item Effect of surface roughness on metal/quenchant interfacial heat transfer and evolution of microstructure(Elsevier Ltd, 2007) Prabhu, K.N.; Fernandes, P.In the present work, the effect of surface roughness on heat transfer rates in various quenchants was determined. The heat flux transients at the probe/quenchant interface were estimated by inverse modeling of heat conduction during end quenching of stainless steel probes with three different surface roughness (grooved, Ra = 3.0 and 1 ?m). Heat transfer during quenching was correlated with the hardness obtained for medium carbon AISI 1060 steel specimens. The effect of surface roughness on heat transfer rate during quenching in water and brine was significant for rough surface whereas its effect on heat transfer rate is only marginal in high viscosity oil quenchants. A fully martensitic structure was observed with grooved surface subjected to water quenching. With a smooth surface a mixed microstructure was obtained. The oil quenched specimens were found to be less sensitive to surface roughness. © 2005 Elsevier Ltd. All rights reserved.Item Effect of section size and agitation on heat transfer during quenching of AISI 1040 steel(2007) Fernandes, P.; Prabhu, K.N.In the present work an attempt has been made to determine the heat flux transients during quenching of Ø28 mm × 56 mm height and Ø44 mm × 88 mm height AISI 1040 steel specimens during lateral quenching in brine, water, palm oil and mineral oil. The heat flux transients were estimated by inverse modeling of heat conduction. The variation of heat flux transients with surface temperature for different quenching media is investigated. Higher peak heat flux transients are obtained for 28 mm diameter specimen than 44 mm diameter specimen during quenching in aqueous media. However quenching with oil media shows opposite results. Agitation of quenching medium increases the peak heat flux during the quenching of steel specimen in all the quenching media. Peak hardness is obtained at the surface and with smaller diameter specimens during agitation. © 2006 Elsevier B.V. All rights reserved.Item Nanoquenchants for industrial heat treatment(2008) Prabhu, K.N.; Fernades, P.The present work outlines the possibility of using nanofluids for industrial heat treatment. Development of nanoquenchants having (i) high quench severity for enhancement of heat transfer for thick sections with low quench sensitivity and (ii) low cooling severity for thin sections with high quench sensitivity would be extremely useful to the heat treating community. The temperature dependent heat transfer coefficient and the wettability of the medium are the two important parameters that can be used to characterize a nanoquenchant to assess its suitability for industrial heat treatment. © 2007 ASM International.Item Design and synthesis of new donor-acceptor type conjugated copolymers derived from thiophenes(2009) Manjunatha, M.G.; Vasudeva Adhikari, A.V.; Hegde, P.K.A new series of donor-acceptor type poly(thiophene) derivatives (P1-P3) were synthesized starting from thiodiglycolic acid and diethyl oxalate through multistep reactions. In the final step, the polymerization was carried out using Wittig reaction. This is a good synthetic route for the preparation of any desired p- and n-type copolymers. The optical and potential charge-transporting properties of the copolymers were investigated by UV-vis, fluorescence emission spectroscopy and cyclic voltammetry. The copolymers exhibited bluish-green/green fluorescence in their thin film forms. Cyclic voltammetry experiments showed that these copolymers have low-lying LUMO energy levels ranging from -2.98 to -3.11 eV and high lying HOMO energy levels ranging from -5.45 to -5.65 eV. The optical and electrochemical studies reveal that new copolymers are new promising materials for the development of efficient polymer light emitting diodes. © 2008 Elsevier Ltd. All rights reserved.Item Severity of quenching and kinetics of wetting of nanofluids and vegetable oils(2009) Jagannath, V.; Prabhu, K.N.In the present work, the suitability of vegetable oil blends with mineral oil and alumina based nanofluids as quench media for industrial heat treatment was investigated. Sunflower oil, palm oil, and mineral oil were used for preparing the blends. Alumina based nanofluids of varying concentrations ranging from 0.01-4 % were used. The size of alumina particles was about 50 nm. The severity of quenching and heat transfer coefficients were estimated during quenching of copper probes. Heat transfer coefficients were estimated using a lumped heat capacitance model. The static contact angle was measured on copper substrates having a surface texture similar to the probes used for estimation of heat transfer coefficients. A dynamic contact angle analyzer was used for this purpose. The measured contact angles of nanofluids on copper were high compared to oils, indicating poor wetting by quench media that are polar in nature. Wetting characteristics had a significant effect on heat transfer coefficients estimated during quenching. Copyright © 2009 by ASTM International.