Journal Articles
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Item Studies on concrete cylinders subjected to elevated temperatures(2010) Babu Narayan, K.S.; Anil Kumar, G.; Chandrakala, C.; Shashikumar, H.M.; Venkataramana, K.; Yaragal, S.C.; Chinnagiri Gowda, H.C.; Reddy, G.R.; Sharma, A.Concrete is a poor conductor of heat, but can suffer considerable damage when exposed to fire. Concrete in structures is likely to be exposed to high temperatures during fire. The relative properties of concrete after such an exposure are of great importance in terms of the serviceability of buildings. Unraveling the heating history of concrete is important to forensic research or to determine whether a fire exposed concrete structures and its components are still structurally sound or not. Assessment of fire damage concrete structures usually starts with visual observation of color change, cracking and spalling. On heating, a change in color from normal to pink is often observed and this is useful since it coincides with the onset of significant loss of concrete strength. This work reports the characteristics of concrete at elevated temperatures. Popular normal strength grades (M20, M25, M30, M35, M40 and M45) produced by Ready Mix Concrete (RMC) India, Mangalore have been used in production of test specimens (150 mm diameter and 300mm height cylinders) to obtain more meaningful and realistic data. In the preliminary phase 150 mm diameter and 300mm height cylinders were cast, cured and tested by destructive method for gathering data on strength characteristics. Later these test samples were subjected to elevated temperatures ranging from 100°C to 800°C, in steps of 100°C with a retention period of 2 hours. After exposure, weight losses were determined and then again destructive tests were conducted to estimate the residual split tensile strength. Test results indicated that weight and strength significantly reduces with an increase in temperature. © 2010 CAFET-INNOVA TECHNICAL SOCIETY. All rights reserved.Item Strength retention characteristics of concrete cubes subjected to elevated temperatures(2010) Yaragal, S.C.; Clarke, K.S.; Mahesh Babu, K.; Ashokumar, S.; Venkataramana, K.; Babu Narayan, K.S.; Chinnagiri Gowda, H.C.; Reddy, G.R.; Sharma, A.Concrete in structures is likely to be exposed to high temperatures during fire. The relative properties of concrete after such an exposure are of great importance in terms of the serviceability of buildings. The probability of its exposure to elevated temperatures is high due to natural hazards, accidents and sabotages. Therefore, the performance of concrete during and after exposure to elevated temperature is a subject of great interest to the designer. Physical changes like cracking, colour change, spalling and chemical changes like decomposition of Ca(OH)2 and the C-S-H gel take place when subjected to elevated temperatures. This work reports the characteristics of concrete at elevated temperatures. Popular normal strength grades (M20, M25, M30, M35, M40 and M45) produced by Ready Mix Concrete (RMC) India, Mangalore have been used in production of test specimens (150 mm cubes) to obtain more meaningful and realistic data. In the preliminary phase 150 mm cubes were cast, cured and tested by destructive method for gathering data on strength characteristics. Later these test samples were subjected to elevated temperatures ranging from 100°C to 800°C, in steps of 100°C with a retention period of 2 hours. After exposure, weight losses were determined and then again destructive tests were conducted to estimate the residual compressive strength. Test results indicated that weight and strength significantly reduces with an increase in temperature. © 2010 CAFET-INNOVA TECHNICAL SOCIETY.Item Studies on normal strength concrete cubes subjected to elevated temperatures(2010) Yaragal, S.C.; Babu Narayan, K.S.; Venkataramana, K.; Kulkarni, K.S.; Gowda, H.C.C.; Reddy, G.R.; Sharma, A.Concrete in structures is likely to be exposed to high temperatures during fire. The probability of its exposure to elevated temperatures is high due to natural hazards, accidents and sabotages. Therefore, the performance of concrete during and after exposure to elevated temperature is a subject of great importance and interest to the designer. Popular normal strength grades of concrete produced by Ready Mix Concrete (RMC) India, Mangalore have been used in production of test specimens (150 mm cubes), cured and tested by destructive method for gathering data on strength characteristics. Later, these test samples were subjected to elevated temperatures ranging from 100 C to 800 C, in steps of 100 C with a retention period of 2 hours. After exposure, weight losses and the residual compressive strength retention characteristics are studied. Test results indicated that weight and strength significantly reduces with an increase in temperature. Residual compressive strength prediction equations are proposed for normal strength concretes subjected to elevated temperatures.Item High temperature performance of self-compacting high-volume fly ash concrete mixes(2011) Amrutha; Nayak, G.; Narasimhan, M.C.; Rajeeva, S.V.Quite often, concrete in structures is likely to get exposed to high temperatures, including an incident of fire. The strength-retention properties of concrete after such an exposure are of great importance in terms of the serviceability of buildings. This paper presents an experimental study on the strength retention and impermeability aspects of a set of self compacting, high-volume fly ash concrete mixes under elevated temperatures. Five selfcompacting concrete mixes with a higher 60% level of cement replacement with fly-ash, are designed and the effects of elevated temperatures, in the range of 200-800 C, on the physical, mechanical and durability properties of these mixes are assessed. The assessment is in terms of the weight losses and the reduction in the compressive strengths of concrete cubes and split tensile strengths of concrete cylinders. The durability characteristics are assessed in terms of RCPT test results on these mixes. Performances of these self compacting concrete mixes (SCC) at elevated temperatures are also compared with two normally-vibrated concrete mixes (NCs) of an equivalent M30 strength grade. Test results indicate that weight of the specimens significantly get reduced with an increase in the level of elevated temperature, with sharp variations beyond 600 C. The experimental results also show that large improvements against chloride-ion penetration and better strength-retention at higher temperatures can be realized with self-compacting high-volume fly-ash concrete mixes additionally admixed with GGBFS and silica fume.Item Fabrication and high-temperature structural characterization study of porous anodic alumina membranes(2012) Choudhari, K.S.; Sudheendra, P.; Udayashankar, N.K.Porous anodic alumina (PAA) membranes with highly ordered array of nanopores were prepared by twostep anodization process. Studies on structural and thermal properties and the thermal stability of the prepared PAA membranes were carried out. Investigation using scanning electron microscopy, atomic force microscopy, X-ray diffraction, thermal analysis and infrared spectroscopy was performed on the prepared PAA membranes at room temperature and in the temperature range 600-1,400 °C. The as-prepared PAA membranes revealed the amorphous nature. Polycrystalline PAA membranes were obtained by annealing carried out at different temperatures. Annealing study confirmed that the heat treatment transformed the amorphous PAA membranes to their crystalline phases, namely, ?-alumina at about 870 °C and then to ?-alumina around 1,250 °C. © Springer Science+Business Media, LLC 2011.Item Diluted magnetism in Mn-doped SrZnO2 single crystals(American Institute of Physics Inc., 2013) Rahman, M.R.; Koteswararao, B.; Huang, S.H.; Kim, K.; Chou, F.C.We have investigated the magnetic properties of Mn- and Cu-substituted SrZnO2 single crystals (SrZn1-xMnxO2 and SrZn1-xCuxO2). We observed signatures of weak ferromagnetism as a sharp increase of magnetic susceptibility below 5 K even in the low-percentage (x = 0.01) of Mn-substituted single crystals. Magnetic susceptibility data measured parallel or perpendicular to the ab-plane yield anisotropic behavior with Curie-Weiss temperature of about -320 K and -410 K, respectively, suggesting the presence of strong antiferromagnetic couplings among Mn at high temperatures, similar to the Mn-doped ZnO and Fe-doped BaTiO3. In contrast, the SrZn0.99Cu0.01O 2 crystal shows paramagnetic behavior down to 2 K. © 2013 AIP Publishing LLC.Item Design and fabrication of spectrally selective TiAlC/TiAlCN/TiAlSiCN/TiAlSiCO/TiAlSiO tandem absorber for higherature solar thermal power applications(Elsevier, 2015) Jyothi, J.; Chaliyawala, H.; Srinivas, G.; Nagaraja, H.S.; Barshilia, H.C.A new nanostructured TiAlC/TiAlCN/TiAlSiCN/TiAlSiCO/TiAlSiO tandem absorber has been designed for higherature solar thermal power applications. The first three layers in this tandem act as an absorbing layer, whereas, TiAlSiCO and TiAlSiO act as semi-transparent and anti-reflecting layers. The tandem absorber was deposited on stainless steel substrates using a four-cathode reactive direct current unbalanced magnetron sputtering system. The composition and thicknesses of the individual component layers have been optimized by adjusting the reactive flow rate of C2H2, N2, O2, and also Al, Ti and Si target power densities to achieve high absorptance (0.961) and low emittance (0.07 at 82 °C). The reflectance data showed that the absorptance increases gradually with shift of reflectance minimum to higher wavelengths from first layer to last layer (i.e., TiAlC to TiAlSiO). The thickness of optimized tandem absorber was calculated from the cross-sectional field-emission scanning electron microscopy images and confirmed using transmission electron microscopy. The performance evaluation of the tandem absorber has been evaluated by heating it in air and vacuum under cycling conditions at different temperatures. These results showed that the tandem absorber was stable up to 325 °C in air for 400 h and up to 650 °C in vacuum for 100 h, thus demonstrating its suitability for higherature solar thermal power generation applications. © 2015 Elsevier B.V. All rights reserved.Item Hydrogen-Economic Synthesis of Gasoline-like Hydrocarbons by Catalytic Hydrodecarboxylation of the Biomass-derived Angelica Lactone Dimer(Wiley Blackwell info@wiley.com, 2017) Chang, F.; Dutta, S.; Mascal, M.The biomass-derived platform molecule levulinic acid is converted into the angelica lactone dimer (ALD) in high overall yield using simple inorganic catalysts. Hydrodecarboxylation of ALD using a Pd/?-Al2O3 catalyst under moderate hydrogen gas pressure at high temperatures generates branched C8–C9 hydrocarbons in nearly quantitative yield consuming as little as a single equivalent of external hydrogen. These molecules are high-octane “drop-in” equivalents of isoalkanes used in commercial gasoline. Catalytic hydrodecarboxylation is presented as a highly effective means to reduce hydrogen demand in biomass-to-biofuel conversion technologies. © 2017 Wiley-VCH Verlag GmbH & Co. KGaA, WeinheimItem Measurement of high temperature emissivity and photothermal conversion efficiency of TiAlC/TiAlCN/TiAlSiCN/TiAlSiCO/TiAlSiO spectrally selective coating(Elsevier B.V., 2017) Jyothi, J.; Soum-Glaude, A.; Nagaraja, H.S.; Barshilia, H.C.A spectrally selective TiAlC/TiAlCN/TiAlSiCN/TiAlSiCO/TiAlSiO coating was deposited on stainless steel substrate by unbalanced magnetron sputtering system. Each individual layer of the tandem absorber was optimized by varying the reactive gas flow rates (C2H2, N2 and O2) and target power densities (Ti, Al and Si). The optimized tandem absorber shows a solar absorptance of 0.960 and an emittance of 0.15 at 82 °C, measured using solar spectrum reflectometer and emissometer, respectively. In order to study the optical properties of the deposited tandem absorber at high operating temperatures the reflectance spectra of the tandem absorber were measured at temperatures ranging from 80 °C to 500 °C by UV–Vis–NIR spectrophotometer and FTIR spectrometers. The reflectance spectra of the as-deposited sample and after high temperature reflectance measurements did not show any significant changes. The thermal emittance of the tandem absorber at high temperatures (80–500 °C) was studied in detail. At the temperature of 200 °C, 300 °C, 400 °C and 500 °C the tandem absorber shows the emittance of 0.152–0.157, 0.181–0.19, 0.214–0.246 and 0.251–0.275, respectively with an absorptance of ~0.930. These results show the good selectivity of the tandem absorber even at high operating temperatures (e.g., 500 °C) with a photothermal conversion efficiency of 88%, thus demonstrating that the tandem absorber is suitable for solar thermal power generation applications. Reflectance and roughness data of the absorber coating post annealing in air up to 600 °C for 2 h, carried out independently, corroborated the present results. © 2017 Elsevier B.V.Item HVOF sprayed Ni3Ti and Ni3Ti+(Cr3C2+20NiCr) coatings: Microstructure, microhardness and oxidation behaviour(Elsevier Ltd, 2018) Reddy, N.C.; Kumar, B.S.A.; Reddappa, H.N.; Ramesh, M.R.; Koppad, P.G.; Kord, S.This paper reports the development of Ni3Ti and Ni3Ti+(Cr3C2+20NiCr) coatings on AISI 420 stainless steel (MDN-420) and titanium alloy ASTM B265 (Ti-15) by HVOF technique. Microstructure, microhardness and high temperature oxidation behaviour of coatings were investigated. Microstructure of coatings was dense and displayed layers depicting lamellar structure. The microhardness of coatings was significantly higher than that of substrate owing to higher density and cohesive strength between individual splats of coating materials. Cyclic oxidation studies conducted on Ni3Ti and Ni3Ti+(Cr3C2+20NiCr) coatings showed oxide scale was composed of various oxides like NiO, NiCr2O4 and Cr2O3 phases. The formation of compact and protective NiO phase in case of Ni3Ti coatings; NiO and Cr2O3 phases in Ni3Ti+(Cr3C2+20NiCr) coatings stabilised the weight gain exhibited slow oxidation rate at higher temperatures. © 2017 Elsevier B.V.