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Item Applications of reinforcement particles in the fabrication of Aluminium Metal Matrix Composites by Friction Stir Processing - A Review(EDP Sciences, 2022) Adiga, K.; Herbert, M.A.; Rao, S.S.; Shettigar, A.Composite materials possess advantages like high strength and stiffness with low density and prove their essentiality in the aviation sector. Aluminium metal matrix composites (AMMC) find applications in automotive, aircraft, and marine industries due to their high specific strength, superior wear resistance, and lower thermal expansion. The fabrication of composites using the liquid phase at high temperature leads to the formation of intermetallics and unwanted phases. Friction Stir Processing (FSP) is a novel technique of composite fabrication, with temperature below the melting point of the matrix, achieving good grain refinement. Many researchers reported enhancement of mechanical, microstructure, and tribological properties of AMMC produced by the FSP route. The FSP parameters such as tool rotational speed, tool traverse speeds are found to be having greater impact on uniform dispersion of particles. It is observed that the properties such as tensile strength, hardness, wear and corrosion resistance, are altered by the FSP processes, and the scale of the alterations is influenced significantly by the processing and tool parameters. The strengthening mechanisms responsible for such alterations are discussed in this paper. Advanced engineering materials like shape memory alloys, high entropy alloys, MAX phase materials and intermetallics as reinforcement material are also discussed. Challenges and opportunities in FSP to manufacture AMMC are summarized, providing great benefit to researchers working on FSP technique. ©Item A comprehensive review of friction stir techniques in structural materials and alloys: challenges and trends(Elsevier Editora Ltda, 2022) Prabhakar, D.A.P.; Shettigar, A.; Herbert, M.A.; Gowdru Chandrashekarappa, M.; Pimenov, D.Y.; Giasin, K.; Prakash, C.Friction-stir techniques are the potential alternative to fusion-based systems for processing and welding metallic alloys and other materials. This review explores the advantages, applications, limitations, and future directions of seven friction-based techniques namely, Additive Friction Stir Deposition (AFSD), Friction Stir Additive Manufacturing (FSAM), Friction Stir Welding (FSW), Friction Stir Processing (FSP), Friction Surfacing (FS), Friction Stir Spot Welding (FSSW), and Friction Stir Lap Welding (FSLW). The basic underlying principle of these processes uses friction as a thermal energy source to weld/process/deposit materials. The common control parameters of all friction stir processing techniques are axial force, rotational speed, and weld or traverse speed. In addition, tool profiles and tool dimensions are known to influence the weld quality. The tool's rotational speed and axial force generate friction between the workpiece and tool material interface, which could plasticize the material. The additive powder bed friction stir process (APBFSP) is another new solid-state manufacturing technique that focus on fabricating the polymer matrix nanocomposites (PNC). In this, a hollow tool like AFSD and the fundamental principle of FSP are combined. The said parameters affect the quantity of material getting deposited/welded. However, weld speed/traverse speed alters the weld quality, and higher traverse speed results in porosity and voids in the welded/deposited/processed region. The only difference between AFSD and other friction stir techniques (FSTs) is that in the AFSD technique, the hollow rotating tool comprises two protrusions with different tool profiles (cylindrical, threaded cylindrical, and tapered cylindrical, square) used. Threaded cylindrical profile and tool steel as the tool material is the most commonly employed in FSTs. Apart from that, tungsten carbide is preferred for hard materials. The working principles and process parameters of FSTs that affect the part quality are discussed in detail. The above review gives the reader an understanding of the domain of FSTs that can be researched further. A summary of some of the potential research works with objectives, process parameters, and outcomes is highlighted. This will provide the readers with an overview of the work carried out by researchers across the globe. Finally, the potential research gaps for future directions to be explored soon across the globe are outlined. © 2022 The Author(s).Item Investigating Mechanical and Corrosion Behavior of Plain and Reinforced AA1050 Sheets Fabricated by Friction Stir Processing(Springer, 2020) Vinayak, V.R.; Bajakke, P.A.; Jambagi, S.C.; Chavana, C.; Deshpande, A.S.The present investigations help in improving the bendability and corrosion resistance of AA1050 rolled sheets by selective friction stirring. The processing of AA1050 with a tapered square pin at a tool rotation speed of 1200 rpm yielded the highest strain of 0.345 at ultimate tensile strength compared with 0.054 in as-received material. The identified processing conditions produced an ultimate tensile strength of 89.23 MPa with a toughness of 34.451 × 106 J/m3 and a lower corrosion rate with Icorr of 0.324 × 10?6 A/cm2. Further, processing with a simple tapered circular pin resulted in maximum ultimate tensile strength of 102 MPa with a toughness of 33.990 × 106 J/m3. However, it came at the expense of least resistance to corrosion with Icorr of 4.813 × 10?6 A/cm2. Consequently, the addition of zinc oxide during friction stirring showed a remarkable improvement in corrosion resistance with Icorr of 0.094 × 10?6 A/cm2. Future studies are planned on these lines. © 2020, The Minerals, Metals & Materials Society.Item Corrosion behavior of novel AA1050/ZnO surface composite: A potential material for ship hull(Elsevier B.V., 2020) Bajakke, P.A.; Vinayak, V.R.; Jambagi, S.C.; Deshpande, A.S.Friction stir processing is one of the effective surface treatments which was employed to process the AA1050 sheets in bare and reinforced condition. The primary objective of the investigation was to expand the applications of AA1050 as a ship hull element in shipbuilding with the least corrosion rate to withstand the harsh marine environment. The base material processed with a rotational speed of 1200 rpm resulted in the highest corrosion rate of 0.173622 mpy. The formation of Al-Fe intermetallic phases was responsible for pitting corrosion. Further, processing by embedding zinc oxide with a rotational speed of 1000 rpm exhibited ~6.68 times improvement in corrosion resistance compared to as-received material. The corrosion rate was found to be 0.003390 mpy. The Al2O3 passive film hinders the initiation and propagation of pits. This study coins a novel composite material and future investigations are emphasized on the same lines. © 2020 Elsevier B.V.Item Tailoring surface characteristics of bioabsorbable Mg-Zn-Dy alloy using friction stir processing for improved wettability and degradation behavior(Elsevier Editora Ltda, 2021) Rokkala, U.; Bontha, S.; Ramesh, M.R.; Balla, V.K.; Srinivasan, A.; Kailas, S.V.Magnesium (Mg) and its alloys are currently under consideration for use as temporary implants. However, early degradation and maintaining mechanical integrity is a significant concern. Surface modification techniques are used to improve mechanical and corrosion properties of Mg based alloys. In the present study, friction stir processing (FSP) was used to tailor the surface characteristics of Mg-1Zn-2Dy (wt.%) alloy for temporary implant applications. The FSPed alloy was characterized using EBSD to understand the influence of FSP on crystallographic texture, grain size and grain boundaries and thereby their effect on corrosion, wettability and hardness. Results showed that the grain size of stir zone (SZ) was refined to less than 3 ?m, as a result of dynamic recrystallization (DRX) during FSP and the FSPed alloy exhibited better wettability than as-cast alloy. An increase in the hardness (11.7%) and elastic modulus (6.84%) of FSPed alloy were also observed. Electrochemical corrosion and weight loss methods were conducted in Dulbecco's Modified Eagle's Medium (DMEM) with, 10% Fetal Bovine Serum (FBS) physiological solution. The lower degradation rate (0.72 mm/yr) of FSPed alloy has been attributed to the fine grains and evenly distributed secondary phase particles. Further, the influence of grain boundary characteristics and crystallographic texture on the corrosion behavior have been investigated. © 2021 The Author(s).Item Comparative investigation of coating and friction stir processing on Mg-Zn-Dy alloy for improving antibacterial, bioactive and corrosion behaviour(Elsevier B.V., 2021) Rokkala, U.; Jana, A.; Bontha, S.; Ramesh, M.R.; Balla, V.K.Magnesium based alloys are well-known materials for temporary implant applications. However, failures due to early degradation and bacterial infection are limiting their applications. To overcome these problems, in the present work a Mg-Zn-Dy alloy based composite surface was prepared using coating and friction stir processing (FSP) techniques. Herein, hydroxyapatite (HA) and silver (Ag) particles were deposited on Mg-Zn-Dy alloy to obtain HA and Ag coated surface (C-HAg). Later, FSP was carried out on the C-HAg surface to develop a Mg-Zn-Dy alloy based composite surface (F-HAg). Field emission scanning electron microscope (FESEM) and energy dispersive X-ray analysis (EDS) confirm the mixing of HA and Ag particles with the Mg-Zn-Dy substrate. Antibacterial studies reveal that both C-HAg and F-HAg samples inhibit Escherichia coli and Staphylococcus aureus bacteria. In vitro cytotoxicity study indicates that the both samples are non-toxic in nature. Results of in vitro corrosion study reveal a significant reduction (72%) in corrosion rate of F-HAg sample when compared to C-HAg sample. The F-HAg samples showed simultaneous improvement in corrosion resistance and antibacterial properties with good biocompatibility. The results of this study indicate that the developed composite surface is a promising material for antibacterial and biodegradable implant applications. © 2021 Elsevier B.V.Item Influence of friction stir processing on microstructure, mechanical properties and corrosion behaviour of Mg-Zn-Dy alloy(Springer, 2023) Rokkala, U.; Bontha, S.; Ramesh, M.R.; Balla, V.K.In the present study, friction stir processing (FSP) was carried out on as-cast Mg-Zn-Dy alloy to tailor grain size and texture which alter the mechanical properties and corrosion behaviour. The grain size of the as-cast alloy was reduced from 60 ± 2 µm to 3 ± 0.1 µm after FSP due to dynamic recrystallization. The effect of grain size, crystallographic orientation and fine precipitates on mechanical properties were investigated using field emission scanning electron microscope (FESEM) and electron back scattered diffraction (EBSD). The ultimate tensile strength, yield strength, % elongation and hardness of FSPed alloy improved by 55%, 60%, 53% and 46% when compared to as-cast alloy. The FSPed Mg-Zn-Dy alloy exhibited a 79% decrease in corrosion rate when compared to as-cast alloy which can be attributed to grain refinement, uniform distribution of secondary precipitates and strong basal texture. The surface of FSPed sample after immersion corrosion exhibited calcium phosphate rich minerals which help in apatite formation on the sample surface. Cytotoxicity studies using MTT assay revealed more than 80% cell viability for both as-cast and FSPed alloy illustrating non-toxic nature of both the samples. The results of this study indicate that FSPed Mg-Zn-Dy alloy is a potential material for biodegradable implants due to its high strength, corrosion resistance and biocompatibility. Graphical Abstract: [Figure not available: see fulltext.]. © 2023, The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature.Item Comparative Study of Plasma Spray and Friction Stir Processing on Wear Properties of Mg-Zn-Dy Alloy(Springer, 2024) Rokkala, U.; Gudala, S.; Ramesh, M.R.Mg alloys are becoming increasingly popular as lightweight materials in recent years. Wear resistance, on the other hand, is a severe issue with Mg alloys. Plasma spray and friction stir processing (FSP) are being investigated in this context for developing composite surfaces with improved surface characteristics. Scanning electron microscopy (SEM), energy dispersive spectroscopy, and x-ray diffraction are used to examine the microstructural changes and phase changes of all materials. After FSP, SEM analysis indicated that the coated particles were equally dispersed throughout the Mg matrix. The composite samples had the lowest wear rate as compared to other samples, according to the wear tests. In comparison to AC, the F-1 sample surface has much higher wear resistance. As a consequence, the findings of this investigation for the F-1 sample appear encouraging for biological wear resistant applications. © ASM International 2023.Item Enhancing wear resistance of AZ61 alloy through friction stir processing: experimental study and prediction model(Institute of Physics, 2024) Anne, G.; Ramesh, S.; Sharma, P.; Maruthi Prashanth, B.H.; Aditya Kudva, S.; Kumar, P.; Sahu, S.; Bhat, N.In this study, friction stir processing (FSP) is proposed for the treatment of AZ61 alloy, and an artificial neural network is built to predict and compare the experimental wear results. The effects of different processing parameters, including spindle speed (800-1200 rpm), traveling speed (5-15 mm min−1), and depth of press (0.8-1.2 mm) on the microstructural evolution, mechanical properties, and wear behavior are investigated. Microstructural analysis reveals a grain size of 14 ± 2 μm for the FSP1 sample, with observed shifting of x-ray diffraction (XRD) peaks, indicative of texture development. Increasing spindle and traveling speeds increase the surface roughness, as observed by average roughness (Ra) values of 68.4 nm for a rotational speed of 800 rpm, traveling speed of 5 mm min−1, and shoulder depth of 0.8 mm (FSP1) and 116.3 nm for rotational speed of 1200 rpm, traveling speed of 15 mm min−1, and shoulder depth of 1 mm (FSP9). Microhardness values increase to 113.36 Hv for FSP1 and 79. 51 Hv for FSP9 compared to 65.92 Hv for the base material (BM) sample. The decrement in hardness from FSP1 to FSP9 can be attributed to increased heat input, resulting in coarse microstructure. Wear results show that FSP1 exhibits the lowest weight loss (0.003 g) and coefficient of friction (COF) (0.28) compared to other FSP conditions and BM samples (weight loss of 0.022 g and COF of 0.68). This work demonstrates the efficacy of friction stir processing in enhancing the wear resistance of magnesium alloys. © 2024 The Author(s). Published by IOP Publishing Ltd.Item Multi-step fabrication of bioactive Mg–Zn–Dy–AlO3/HA composites: exploring the synergistic effects of plasma spray and friction stir processing(Springer, 2024) Rokkala, U.; Bontha, S.; Ramesh, M.R.; Balla, V.K.Magnesium (Mg) alloys are gaining more attention in recent times as biodegradable materials. However, two major problems with Mg alloy implants are bacterial infections and poor corrosion resistance. In this context, a composite surface (Mg–Zn–Dy–Al2O3/HA) is developed using surface modification techniques. First, Al2O3 + HA composite powder is coated on Mg–Zn–Dy alloy to attain coated surface (C-AHa). Next, the C-AHa surface is subjected to friction stir processing to develop composite surface (F-AHa). Microstructural characterization reveals that, the Al2O3 + HA particles were distributed evenly into the Mg–Zn–Dy substrate. Antimicrobial activities against Escherichia coli and Staphylococcus aureus reveal low adhesion of bacteria on the F-AHa sample surface due to low surface energy (37.83 ± 0.22 mN/m) and low surface roughness (0.36 ± 0.1 µm). Further, the cytotoxicity tests confirm that the F-AHa sample shows significant improvement in cell viability (98%) after 7 days and non-toxic against the mouse osteoblast cells. In Vitro corrosion study observations demonstrate that the corrosion rate for the F-AHa sample is decreased by 72% compared to the C-AHa sample. Thus, the results of this study for the fabricated composites are promising for antimicrobial, biocompatible and bioabsorbable temporary implants. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2024.