Journal Articles
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Item Heat transfer during quenching of modified and unmodified gravity die-cast A357 cylindrical bars(2006) Prabhu, K.; Hemanna, P.Heat transfer during quenching of chill-cast modified and unmodified A357 Al-Si alloy was examined using a computer-aided cooling curve analysis. Water at 60°C and a vegetable oil (palm oil) were used as quench media. The measured temperatures inside cylindrical probes of the A357 alloy were used as inputs in an inverse heat-conduction model to estimate heat flux transients at the probe/quenchant interface and the surface temperature of the probe in contact with the quench medium. It was observed that modified alloy probes yielded higher cooling rates and heat flux transients. The investigation clearly showed that the heat transfer during quenching depends on the casting history. The increase in the cooling rate and peak heat flux was attributed to the increase in the thermal conductivity of the material on modification melt treatment owing to the change in silicon morphology. Fine and fibrous silicon particles in modified A357 probes increase the conductance of the probe resulting in higher heat transfer rates. This was confirmed by measuring the electrical conductivity of modified samples, which were found to be higher than those of unmodified samples. The ultrasound velocity in the probes decreased on modification. ©ASM International.Item Wetting kinematics and spreading behaviour of water based aluminium nanofluids during immersion quenching(2013) Ramesh, G.; Prabhu, K.In the present work, wetting kinematics of water based aluminium nanofluids having nanoparticle concentrations varying from 0.001 to 0.5 vol.-% during immersion quenching of Inconel 600 probe was investigated by measuring the contact resistance. The contact resistance between the quench probe and counter electrode during quenching indicated that the duration of the film of water vapour decreased with increasing nanoparticle concentration as well as absence of stable vapour film formation with 0.05, 0.1 and 0.5 vol.-% of nanoparticles. The phenomenon of a repeated wetting process was observed during quenching in nanofluids. Further, quenching in 0.1 and 0.5 vol.-% nanofluids indicated the formation of a nanoparticle porous layer and its deposition on the quench probe. The spreading behaviour was studied by measuring the dynamic contact angle of nanofluids droplets on Inconel 600 substrate. Contact angle measurement showed that the addition of aluminium nanoparticles did not have a significant effect on the relaxation of contact angle of water droplet. However, lower static contact angles were obtained for nanofluids indicating improved wetting. © 2013 IHTSE Partnership.Item The effect of addition of copper nanoparticles on wetting behaviour of water during immersion quenching(2013) Ramesh, G.; Prabhu, K.In the present work, the effect of addition of copper nanoparticles to water, in concentrations varying from 0.001-0.1 vol%, on wetting behaviour during immersion quenching of Inconel 600 probe was assessed using near surface temperature probe and contact resistance methods. Quenching in nanofluids resulted in decreased duration of vapour blanket stage and rapid wetting. The wetting front velocity increases with increase in nanoparticle concentration. A stable vapour film was not formed during quenching in nanofluids of 0.05 and 0.1 vol%. Quenching in 0.01, 0.05 and 0.1 vol% nanofluids showed characteristics of repeated wetting process. Quenching in 0.1 vol% nanofluid resulted in the formation of porous layer of nanoparticles. © 2013 Indian Institute of Metals.Item Effect of thermal conductivity and viscosity on cooling performance of liquid quench media(Maney Publishing Suite 1C, Joseph's Well, Hanover Walk Leeds LS3 1AB, 2014) Ramesh, G.; Prabhu, K.In this present work, the effect of the thermophysical properties of quenchants on its cooling performance was investigated. Water, brine solutions, polymer solutions and mineral oils were chosen to have quench media with varying thermophysical properties. Cooling curve analyses were carried out by using standard ISO/DIS 9950 quench probe. Grossmann H quench severity of the quench media was determined from the relation of H and cooling rate. Cooling curve analysis results showed that the change in thermophysical properties of the quench media had significant effect on the cooling history of the quench probe. The viscosity of the quenchant used for immersion quenching is the most important factor that controls the cooling performance of the quenchant compared to thermal conductivity of the quench medium. © 2014 IHTSE Partnership.Item Wetting kinetics, kinematics and heat transfer characteristics of pongamia pinnata vegetable oil for industrial heat treatment(Elsevier Ltd, 2014) Ramesh, G.; Prabhu, K.The suitability of pongamia pinnata vegetable oil as cooling medium for quench heat treatment was investigated. Wetting kinetics, kinematics and heat transfer characteristics of pongamia oil during immersion quenching of hot Inconel probe were determined and compared with palm and mineral oils. A comparison of the relaxation of contact angle indicated early attainment of equilibrium contact angle for pongamia oil droplet on Inconel substrate. The equilibrium contact angle value of pongamia oil was in between mineral and palm oils. However, the spreading kinetics was faster with pongamia oil. Pongamia oil showed the formation of a stable vapour film on the probe surface during quenching. This phenomenon was not observed in palm oil and other vegetable oils reported in literature. Pongamia pinnata oil exhibits uniform nature of wetting front, intermediate rewetting temperature and less variations in rewetting temperatures during quenching. The hardening power of pongamia oil was higher than palm and mineral oils and the cooling of the probe was more uniform during quenching in pongamia oil. The heat transfer characteristics of pongamia oil were found to be superior to palm and mineral oils after film/transition boiling. Pongamia oil showed lower heat transfer but more uniform cooling during film boiling. © 2014 Elsevier B.V.Item Wetting and cooling performance of mineral oils for quench heat treatment of steels(Iron and Steel Institute of Japan, 2014) Ramesh, G.; Prabhu, K.In the present work, wetting kinetics, kinematics and heat transfer characteristics of mineral oils having varying thermo-physical properties sourced from different suppliers were investigated using contact angle, online video imaging and cooling curve analysis techniques. The relaxation behavior of mineral oils of low viscosity and surface tension on Inconel substrate indicated improved wettability and fast spreading kinetics while mineral oils of high viscosity and surface tension showed reduced wettability and slower spreading kinetics. Further, the spreading behavior of mineral oils of lower viscosity and density showed the absence of viscous regime. During rewetting, formation of double wetting fronts and more uniform nature of wetting front were observed with mineral oils of high viscosity and flash point whereas no additional wetting front was observed for mineral oils of low viscosity and flash point. Among the convectional/fast/hot mineral oils, higher wetting front velocity and cooling rate were obtained for low viscosity mineral oil. The heat extracting capability of high viscosity mineral oils was higher during vapour and nucleate boiling and lower during liquid cooling stage. Further, highly viscous mineral oils showed uniform heat transfer compared to mineral oils having low viscosity. © 2014 ISIJ.Item Spatial dependence of heat flux transients and wetting behavior during immersion quenching of inconel 600 probe in brine and polymer media(Springer Boston, 2014) Ramesh, G.; Prabhu, K.Cooling curve analysis of Inconel 600 probe during immersion quenching in brine and polymer quench media was carried out. Thermal histories at various axial and radial locations were recorded using a high-speed data acquisition system and were input to an inverse heat-conduction model for estimating the metal/quenchant heat flux transients. A high performance smart camera was used for online video imaging of the immersion quenching process. Solution to two-dimensional inverse heat-conduction problem clearly brings out the spatial dependence of boundary heat flux transients for a Inconel 600 probe with a simple cylindrical geometry. The estimated heat flux transients show large variation on axial as well as radial directions of quench probe surface for brine quenching. Polymer quenching showed less variation in metal/quenchant heat flux transients. Shorter durations of vapor film, higher rewetting temperatures, and faster movement of wetting front on quench probe surface were observed with brine quenching. Measurement of dynamic contact angle showed better spreading and good wettability for polymer medium as compared to brine quenchant. The solid-liquid interfacial tension between polymer medium and Inconel substrate was lower compared with that of solution. Rewetting and boiling processes were nonuniform and faster on quench probe surface during immersion quenching in brine solution. For the polymer quench medium, slow rewetting, uniform boiling and repeated wetting were observed. © 2014 The Minerals, Metals & Materials Society and ASM International.Item A dimensional parameter for prediction of cooling performance of quenchants(ASTM International, 2014) Prabhu, K.; Ramesh, G.Computer aided cooling curve analysis was carried out during immersion quenching of ISO/DIS 9950 quench probe. Water, brine solutions, polymer solutions, mineral oils, and vegetable oils were used as quench media. The results showed that the quench medium used had a significant effect on the quench probe cooling curve parameters. An empirical correlation was proposed to predict the average cooling rate from surface tension, wetting angle, thermal conductivity, and kinematic viscosity of the quench medium. © 2014 by ASTM International.Item Cooling performance of select mineral oil and polymer quenchants(ASTM International, 2014) Tiwary, V.; Prabhu, K.In the present investigation, quench severity was determined for industrial oil quenchants and varying concentrations of PAG polymer. Viscosity, thermal conductivity, density, flash point, and fire point were measured for all quenchants. Cooling curve parameters were determined based on cooling curve analysis ISO/DIS 9950 technique. An Inconel 600 probe was used for this purpose. Severity of quenching was determined based on the Grossmann technique. Viscosity and thermal conductivity had a significant effect on quench severity. Heat flux and HTC at the metal/quenchant interface were computed by both lumped capacitance and Inverse modeling techniques. The effect of ultrasonic and Tensi agitation on cooling curve parameters was assessed. Polymer quenchants of lower concentrations showed marginally higher heat transfer rates compared to water particularly during unagitated condition. © © 2014 by ASTM International.