Browsing by Author "Tay, F.R."

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Effects of smear layer removal agents on the physical properties and microstructure of mineral trioxide aggregate cement
(2017) Ballal, N.V.; Sona, M.; Tay, F.R.
Objective To compare the effect of QMix (Dentsply Sirona), 7% maleic acid (MA), and 17% ethylenediaminetetraacetic acid (EDTA) on the microhardness, flexural strength and microstructure of mineral trioxide aggregate (MTA; ProRoot MTA, Dentsply Sirona). Methods Forty MTA specimens were divided into four groups: [I] QMix [II] 7% MA [III] 17% EDTA and [IV] distilled water (control). After treatment with 5 mL of the respective solution for 1 min, the specimens were tested for microhardness using a Knoop hardness tester. Forty additional specimens were similarly treated and evaluated for the flexural strength using a universal testing machine. For microstructure evaluation, MTA specimens were treated in a similar manner and examined by X-ray diffractometry and scanning electron microscopy (SEM). Results For microhardness, there were no differences between distilled water, QMix and EDTA groups. However, MTA exposed to distilled water had higher microhardness than MA. When compared with QMix and EDTA, MA had lower microhardness; there was no difference between EDTA and QMix. For flexural strength, distilled water group had higher flexural strength than the other agents. There were no differences between EDTA vs MA and EDTA vs QMix. Specimens treated with QMix had higher flexural strength than MA. X-ray diffraction indicated that EDTA inhibited hydration of MTA. For SEM, all the tested agents altered the microstructure of MTA when compared to distilled water. Conclusion MA had more detrimental effect on the physical properties of MTA and EDTA was more detrimental to the hydration of MTA. Clinical significance The present study highlights the effect of newer chelating agents on the physical properties and microstructure of MTA. Preventing the deterioration of MTA is important for its long term success in endodontic procedures. 2017
Effects of smear layer removal agents on the physical properties and microstructure of mineral trioxide aggregate cement
(Elsevier Ltd, 2017) Nidambur, N.V.; Sona, M.; Tay, F.R.
Objective To compare the effect of QMix (Dentsply Sirona), 7% maleic acid (MA), and 17% ethylenediaminetetraacetic acid (EDTA) on the microhardness, flexural strength and microstructure of mineral trioxide aggregate (MTA; ProRoot MTA, Dentsply Sirona). Methods Forty MTA specimens were divided into four groups: [I] QMix [II] 7% MA [III] 17% EDTA and [IV] distilled water (control). After treatment with 5 mL of the respective solution for 1 min, the specimens were tested for microhardness using a Knoop hardness tester. Forty additional specimens were similarly treated and evaluated for the flexural strength using a universal testing machine. For microstructure evaluation, MTA specimens were treated in a similar manner and examined by X-ray diffractometry and scanning electron microscopy (SEM). Results For microhardness, there were no differences between distilled water, QMix and EDTA groups. However, MTA exposed to distilled water had higher microhardness than MA. When compared with QMix and EDTA, MA had lower microhardness; there was no difference between EDTA and QMix. For flexural strength, distilled water group had higher flexural strength than the other agents. There were no differences between EDTA vs MA and EDTA vs QMix. Specimens treated with QMix had higher flexural strength than MA. X-ray diffraction indicated that EDTA inhibited hydration of MTA. For SEM, all the tested agents altered the microstructure of MTA when compared to distilled water. Conclusion MA had more detrimental effect on the physical properties of MTA and EDTA was more detrimental to the hydration of MTA. Clinical significance The present study highlights the effect of newer chelating agents on the physical properties and microstructure of MTA. Preventing the deterioration of MTA is important for its long term success in endodontic procedures. © 2017
Wettability of root canal sealers on intraradicular dentine treated with different irrigating solutions
(2013) Ballal, N.V.; Tweeny, A.; Khechen, K.; Prabhu, K.N.; Satyanarayan; Tay, F.R.
Objectives The aim of this in vitro study was to evaluate the wettability of AH Plus and ThermaSeal Plus sealers on intraradicular dentine treated with different irrigating solutions. Methods Fifty anterior teeth were decoronated and split longitudinally. Each root half was divided into 5 groups (n = 10). Group I: 5 mL of 2.5% NaOCl + QMix. Group II: 5 mL of 2.5% NaOCl + 17% EDTA. Group III: 5 mL of 2.5% NaOCl + 7% maleic acid. Group IV: 5 mL of 2.5% NaOCl. Group V: 5 mL of distilled water. Irrigation regimens were performed for 1 min. Each specimen was placed inside a Dynamic Contact Angle Analyser. A controlled-volume droplet of sealer was placed on each specimen and the static contact angle was analysed. Results The contact angle made by both sealers with EDTA-irrigated dentine was significantly larger when compared to the other irrigants (P < 0.05). For ThermaSeal Plus, contact angles produced on maleic acid-, NaOCl- and distilled water-irrigated dentine were not significantly different, but were all significantly larger than the contact angle produced on QMix-irrigated dentine (P < 0.05). For AH Plus, contact angles produced on NaOCl- and distilled water-irrigated dentine were not significantly different, but were significantly larger than those made by maleic acid and QMix. Conclusion When used as a final irrigant, QMix favours the wetting of root canal dentine by both AH Plus and ThermaSeal Plus sealers. Maleic acid shows a promising result when compared to EDTA and NaOCl. Wettability of both sealers is the worst on EDTA-irrigated dentine. Clinical significance The present study highlights the effect of newer endodontic irrigating solutions on the wettability of sealers on to the root canal dentine, which is required for obtaining good obturation seal. � 2013 Elsevier Ltd.
Wettability of root canal sealers on intraradicular dentine treated with different irrigating solutions
(2013) Nidambur, N.V.; Tweeny, A.; Khechen, K.; Prabhu, K.; Satyanarayan, S.; Tay, F.R.
Objectives The aim of this in vitro study was to evaluate the wettability of AH Plus and ThermaSeal Plus sealers on intraradicular dentine treated with different irrigating solutions. Methods Fifty anterior teeth were decoronated and split longitudinally. Each root half was divided into 5 groups (n = 10). Group I: 5 mL of 2.5% NaOCl + QMix. Group II: 5 mL of 2.5% NaOCl + 17% EDTA. Group III: 5 mL of 2.5% NaOCl + 7% maleic acid. Group IV: 5 mL of 2.5% NaOCl. Group V: 5 mL of distilled water. Irrigation regimens were performed for 1 min. Each specimen was placed inside a Dynamic Contact Angle Analyser. A controlled-volume droplet of sealer was placed on each specimen and the static contact angle was analysed. Results The contact angle made by both sealers with EDTA-irrigated dentine was significantly larger when compared to the other irrigants (P < 0.05). For ThermaSeal Plus, contact angles produced on maleic acid-, NaOCl- and distilled water-irrigated dentine were not significantly different, but were all significantly larger than the contact angle produced on QMix-irrigated dentine (P < 0.05). For AH Plus, contact angles produced on NaOCl- and distilled water-irrigated dentine were not significantly different, but were significantly larger than those made by maleic acid and QMix. Conclusion When used as a final irrigant, QMix favours the wetting of root canal dentine by both AH Plus and ThermaSeal Plus sealers. Maleic acid shows a promising result when compared to EDTA and NaOCl. Wettability of both sealers is the worst on EDTA-irrigated dentine. Clinical significance The present study highlights the effect of newer endodontic irrigating solutions on the wettability of sealers on to the root canal dentine, which is required for obtaining good obturation seal. © 2013 Elsevier Ltd.