Browsing by Author "Bodhak, S."
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Item Material extrusion additive manufacturing of bioactive glass/high density polyethylene composites(Elsevier Ltd, 2021) Jeyachandran, P.; Bontha, S.; Bodhak, S.; Balla, V.K.; Doddamani, M.Bioactive glasses (BAG) are renowned for their unique ability to bond with tissues and therefore are used extensively for bone repair and functional recovery. In this work, high density polyethylene (HDPE) reinforced with BAG is processed using material extrusion additive manufacturing (MEAM) for potential orthopaedic applications. The constituents are melt compounded by varying BAG proportions (5, 10, and 20 wt %) and subsequently extruded into filaments. DSC curves show an insignificant change in the peak melting temperature, increase in crystallization temperature, and a decrease in the crystallinity of HDPE with BAG addition. Warpage analysis confirms that the enhanced temperature parameters and BAG addition result in reduced warpage and improved dimensional stability. Rheological results show that the addition of BAG increases complex viscosity, storage and loss modulus. Melt behavior and print parameters are tailored to improve first layer adhesion and interfacial bonding rendering dimensionally stable prints without any print induced defects. Dynamic mechanical analysis (DMA) of printed samples show an increase in storage (E?), loss (E?) modulus, and a decrease in damping factor (Tan ?) with BAG addition. MEAM of the developed H/BAG composites shows a strong potential for developing customizable scaffolds and implants as bone replacements. © 2021 Elsevier LtdItem Mechanical behaviour of additively manufactured bioactive glass/high density polyethylene composites(Elsevier Ltd, 2020) Jeyachandran, P.; Bontha, S.; Bodhak, S.; Balla, V.K.; Kundu, B.; Doddamani, M.Bioactive glass (BAG) is a well-known biomaterial that can form a strong bond with hard and soft tissues and can also aid in bone regeneration. In this study, BAG is added to a polymer to induce bioactivity and to realize fused filament fabrication (FFF) based printing of polymer composites for potential orthopaedic implant applications. BAG (5, 10, and 20 wt%) is melt compounded with high density polyethylene (HDPE) and subsequently extruded into feedstock filament for FFF-printing. Tensile tests on developed filaments reveal that they are stiff enough to resist forces exerted during the printing process. Micrography of printed HDPE/BAG reveals perfect diffusion of raster interface indicating proper selection of printing parameters. Micrography of freeze fractured prints shows the homogeneous distribution and good dispersion of filler across the matrix. The tensile, flexural, and compressive modulus of FFF-printed HDPE/BAG parts increases with filler addition. BAG addition to the HDPE matrix enhances flexural and compressive strength. The tensile and flexural behaviour of FFF-prints is comparable to injection molded counterparts. Property maps exhibit the merits of present study over the existing literature pertaining to desired bone properties and polymer composites used in biomedical applications. It is envisioned that the development of HDPE/BAG composites for FFF-printing can lead to possible orthopaedic implants and scaffolds to mimic the bone properties in customised anatomical sites or injuries. © 2020 Elsevier LtdItem Quasi-static compressive behavior of bioactive glass reinforced high density polyethylene composites(Elsevier B.V., 2022) Jeyachandran, P.; Bontha, S.; Bodhak, S.; Krishna Balla, V.; Doddamani, M.Compressive behavior of additively manufactured bioactive glass (BAG) reinforced high density polyethylene (HDPE) composites under quasi static conditions (0.001, 0.01 and 0.1 s−1 strain rates) is investigated in this work. HDPE feedstock filaments with 5, 10 and 20 wt% of bioactive glass are extruded for fused filament fabrication (FFF) based 3D printing (3DP). Compressive properties are extracted from the stress–strain plots. Elastic modulus and yield strength of the samples increase with filler addition and strain rate. Energy absorption increases with increase in strain rate and BAG content. All the samples exhibit homogeneous ductile deformation with distinct barrelling effect without any visible cracks. Deformation and energy absorption behavior of the tested samples are investigated using micrography. © 2021 Elsevier B.V.
