Browsing by Author "Bhat, K.U."

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Ag-TiO2 nanoparticles for photocatalytic degradation of lomefloxacin
(Taylor and Francis Inc. 325 Chestnut St, Suite 800 Philadelphia PA 19106, 2016) Kulkarni, R.M.; Malladi, R.S.; Hanagadakar, M.S.; Doddamani, M.R.; Bhat, K.U.
The photocatalytic activity of silver-doped TiO2 (Ag-TiO2) nanoparticles was studied by photocatalytic degradation of lomefloxacin (LMF) using a photoreactor with a mercury lamp (PHILIPS, TUV 8 W T5, Emax = 254 nm). The 1 and 2% silver-doped TiO2 nanoparticles were synthesized by liquid impregnation (LI) method. The resulting nanoparticles were characterized by surface analytical methods such as X-ray diffraction (XRD), scanning electron microscope (SEM), energy dispersive X-ray analysis and transmission electron microscope (TEM). The study shows 2% Ag-TiO2 nanoparticles exhibited better results (95% degradation) in 1 h for the degradation of lomeofloxacin compared to 1% Ag-TiO2 and pure TiO2. XRD analysis indicated that the crystallite size of TiO2 was 17.00 nm, while the crystallite size of 1% Ag-TiO2 and 2% Ag-TiO2 was 13.07 to 14.17 nm. TEM images show the particle size of Ag-TiO2 nanoparticles were in the range 40–45 nm in length and 10–15 nm in breadth. Pseudo-first-order rate constants were found to decrease with increase in pH. The effect of UV intensity, catalyst dosage and initial concentration of LMF on the degradation rate were also studied and elaborately discussed. © 2015 Balaban Desalination Publications. All rights reserved.
Assessment of triboelectricity in colossal-surface-area-lanthanum oxide nanocrystals synthesized via low-temperature hydrothermal process
(Springer, 2021) Meti, S.; Hosangadi Prutvi, H.P.; Rahman, M.R.; Bhat, K.U.
Triboelectric nanogenerators (TENGs) have marked their applications in various fields, most importantly, in medical devices. The electrical output of the TENGs mainly concentrated on parameters such as electrode separation distance, applied mechanical pressure, surface charge density, and overlapping surface area. The surface area of the active layer in TENGs plays a crucial role. Given this, the present contribution is the first report on the utilization of lanthanum oxide (La2O3) as an active material with a large surface area (~ 72.33 m2/g) in TENGs. The nanocrystals of La2O3 have been successfully embedded into TENGs architecture through a high-quality screen-printed film with a Teflon-counter surface. The in-house test-rig of TENGs resulted in an output open-circuit voltage of 120 V and a short-circuit current of 23.7 ?A. Further, the maximum power density is 7.125 W/m2 at an external load resistance of 30 M?. These results suggest that La2O3 is a suitable contender in various self-powered devices. © 2021, The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature.
Beneficial Effect of Manganese(II) Ions on the Morphology of Polyol Synthesised Silver Nanowires
(Korean Institute of Metals and Materials, 2020) Prabukumar, C.; Bhat, K.U.
Abstract: Silver nanowires (Ag NWs) is a potential material to be used as the transparent conductive electrode (TCE) material, in the flexible electronic applications. The polyol method is the commonly used technique to synthesis the silver nanowires. The growth of the silver nanowires is facilitated by the oxidative etching of the silver seed particles. The present work investigates the influence of the manganese(II) ions to promote the growth of silver nanowires. The manganese(II) ions, due to its multiple oxidation states, play an essential role in removing the dissolved atomic oxygen, which prevent the growth of longer nanowires. Its effect on the length and diameter of the silver nanowires is studied in detail with different concentration levels. Characterization tools, such as X-ray diffractometry, electron microscopy (FESEM and TEM) and UV–VIS spectroscopy are used to characterise the synthesised silver nanowires. The addition of manganese(II) ions alters the aspect ratio of the silver nanowires that in turn, affects the optoelectrical properties of the TCE films. By using the synthesised silver nanowires, transparent heaters are successfully fabricated and their performances under different conditions are evaluated. Graphic Abstract: [Figure not available: see fulltext.]. © 2020, The Korean Institute of Metals and Materials.
Biosynthesis of copper nanoparticles using copper-resistant Bacillus cereus, a soil isolate
(Elsevier Ltd, 2016) Tiwari, M.; Jain, P.; Raghu Chandrashekar, R.; Narayanan, K.; Bhat, K.U.; Udupa, N.; Rao, J.V.
Microorganisms are useful systems for the production of biocompatible metal nanoparticles. Copper, an essential element of life, has good therapeutic potential. However, copper lacks suitable form for effective in vivo delivery, which has diminished its applicability. In this study, we produced biosynthesized copper nanoparticles (BCuNps) using a copper-resistant bacterial isolate from copper mine. The organism was able to tolerate >10 mM of copper and when analysed by 16S rRNA technique, showed 100% similarity with Bacillus cereus. BCuNps, produced by this microorganism, in cell-free filtrate, were characterized for surface plasmon resonance (SPR), particle's characteristics, spectroscopic properties and morphology. SPR peaks for BCuNps were recorded between 570–620 and 350–370 nm. BCuNps characteristics, namely particle size distribution, polydispersity index and zeta potential were found to be 11–33 nm, 0.433 and (?) 19.6 mV, respectively. Scanning electron microscope (SEM), transmission electron microscope (TEM) and atomic force microscope (AFM) analyses confirmed the uniform morphology; X-ray diffraction (XRD) spectrum revealed the crystalline nature; and Fourier transform infrared (FTIR) spectrum disclosed the presence of protein with BCuNps. A comparative evaluation of BCuNps with copper sulphate to determine their antimicrobial and cell toxicity levels was undertaken. BCuNps showed better antimicrobial effect and found to be safer against normal cell lines, such as HaCat, Vero and hFOB, than the copper sulphate control. © 2016 Elsevier Ltd
Chemical free synthesis of graphene oxide in the preparation of reduced graphene oxide-zinc oxide nanocomposite with improved photocatalytic properties
(Elsevier B.V., 2018) Meti, S.; Rahman, M.R.; Ahmad, M.I.; Bhat, K.U.
In the present investigation, the reduced graphene oxide – zinc oxide (rGO-ZnO) was prepared by rapid microwave-assisted hydrothermal technique. The chemical free graphene oxide (GO), synthesized by Tang Lau technique, was used in the preparation of rGO-ZnO nanocomposite. The GO gets reduced to rGO during microwave irradiation and provides the necessary nucleation site for the ZnO nanorods to grow in [0 0 0 1] direction. These ZnO nanorods were completely wrapped with rGO sheets, confirmed by the synchrotron XRD and TEM techniques. The phases and cell parameters were calculated by Rietveld method. The prepared composite was used for the photodegradation of methyl orange (MO) dye from water under UV light. Investigation revealed that the incorporation of rGO into the ZnO increased the photodegradation ability of the bare ZnO. The performance of the composite is also compared with the rGO-ZnO nanocomposite, where rGO was prepared by Hummer's method. rGO obtained from Tang Lau method formed stable and efficient composite with ZnO and exhibited higher activity compared to the composite, wherein rGO was prepared from conventional Hummer's method. Under UV light, the ZnO liberates photoelectrons which reacts with surface oxygen to form superoxide radicals (O ? 2 ) and (OH ? ) in the water medium. The rGO nanosheets could reduce the charge recombination during the reaction. The active species adsorbs the MO molecules and degrades into CO 2 , H 2 O and other byproducts. More than 3.5 times increase in the rate constant was observed for rGO-ZnO compared to the bare ZnO. © 2018 Elsevier B.V.
Crystallite size measurement and micro-strain analysis of electrodeposited copper thin film using Williamson-Hall method
(American Institute of Physics Inc. subs@aip.org, 2016) Augustin, A.; Rajendra Udupa, K.; Bhat, K.U.
The improvement in hydrophilicity of copper coating on aluminium for better antimicrobial activity can be achieved by increase in surface energy. The surface energy depends on the micro-strain of the coating. Micro-strain in the coatingincreases with reduction in crystallite size. In this investigation, the crystallite size in the electrodeposited copper coating was varied by varying deposition current density. Crystallite size and micro-strain in the coating were estimated using Williamson-Hall method. Values of crystallite sizes using TEM micrographs were in agreement with that using Williamson-Hall method. Also, presence of nano-Twins in the coating contributed for micro-strain in copper coating. Â© 2016 Author(s).
Cumulative effect of FexN phases, roughness parameters, and asperity geometry on the anti-wear properties of low-temperature plasma nitrided Ti-Nb stabilized IF steel
(Elsevier Ltd, 2025) Sahoo, B.; Bhat, K.U.
Plasma-driven surface modification techniques like plasma nitriding (PN) are trending, especially for steel products. It is advantageous due to the higher order of process control and superior quality of property enhancement of the surface. This technique often employs a high processing temperature, which is one of its metallurgical and economical limitations. One of the renowned solutions is the implementation of lower processing temperatures. The current work is based on the low-temperature plasma nitriding of Ti-Nb stabilized interstitial-free steel at different processing temperatures ranging from 400 ºC to 500 ºC. The role of FexN phases, surface roughness parameters, and asperities geometry are thoroughly studied with respect to the anti-wear properties of the surface. The formation of ??-Fe4N and ?-Fe2–3N are detected in the XRD plot, whereas ??-Fe16N2 is confirmed in microscopy. The sample treated at 450 ºC presents the best anti-wear properties compared to other samples, primarily due to the presence of prominent ?-Fe2–3N phase and blunt surface asperities. A maximum reduction in wear volume of about 3 times the base value is recorded in the wear test. The microscopic and elemental analyses are conducted on the wear scars, wear debris, and counter-body worn-out surfaces to study the wear mechanism comprehensively. The work tries to illustrate the wear mechanisms schematically to understand the conceptual grounds associated with such theories. The spectrometric analysis in the depth direction is also performed, and it detects the trace of nitrogen up to about 7 µm depth for 500 ºC nitriding conditions. © 2025
Damage Tolerance Capability of Retrogression and Re-aged 7010 Aluminum Alloy Under FALSTAFF Loading
(Springer, 2020) Nandana, M.S.; Bhat, K.U.; Manjunatha, C.M.
The present work deals with the damage tolerance characteristics of high strength aluminum alloy tempered in T6 and reversion condition. The fatigue experiments were carried out by applying a service simulating load spectrum, i.e., standard mini FALSTAFF loading. The crack propagation speed was found to be lower and the total crack propagation life was longer by 22% for reversion-treated alloy. The crack growth was also predicted to be using two parameter crack driving force approach. The fatigue data of these treated alloys under constant amplitude loading at various stress ratios were analyzed to obtain crack growth law. The predicted crack growth behavior was conservative and followed similar trend in both the alloys as observed in experiments. Predicted results of reversion-treated alloy also showed longer crack growth life. The modified microstructure after reversion treatment was attributed for the observed improvement in damage tolerance capability. © 2020, The Indian Institute of Metals - IIM.
Development of adherent antimicrobial copper coatings on stainless steel for healthcare applications
(Springer, 2023) Bharadishettar, N.; Bhat, K.U.; Bhat, K.S.
Copper coatings were fabricated using an environmentally sustainable non-cyanide electrodeposition technique. By following four-stage acid pickling treatment of the substrate and optimum parameters during electrodeposition, adhesion strength up to 9 MPa was obtained. Four different copper coatings were fabricated by varying CuSO4. 5H2O concentration in an electrolyte (10, 15, 30, and 45 g/L) to understand nucleation and growth mechanism and surface texture evolution. Nano-nodular morphology of the deposited copper marks a significant feature. It increases the fraction of grain boundaries in it. The grazing incidence X-ray diffraction analysis revealed the preferred orientation along the (111) plane with the presence of residual compressive stresses (in the range of 24.90–273.92 MPa). Surface texture studies indicated that the coating had an abundance of nano-scaled protruding structures with surface roughness’s Sa in the range of 2.507–1.674 µm (Ra in a range of 1.714–1.235 µm). It offers 3D contact with microbes. The developed coating had increased hardness (41.93%), scratch resistance (58.77%), and 9 MPa adhesion strength with the substrate. Initially, copper coatings had hydrophobicity against water (initial contact angle in the range of 134–139°). The extent of hydrophobicity decreased with exposure time. The developed coatings exhibited significant antimicrobial activity. Antimicrobial studies using the cell viability technique indicated that the coating exhibits toxicity against Escherichia coli (ATCC25922) and Staphylococcus aureus (MCC2408) microbes. 100% reduction of the survival of microbes is observed after 4 h of exposure. Graphical Abstract: [Figure not available: see fulltext.]. © 2023, The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature.
Development of nanolaminated multilayer Ni-P alloy coatings for better corrosion protection
(Royal Society of Chemistry, 2016) Elias, L.; Bhat, K.U.; Hegde, A.
Nanolaminated multilayer Nickel-Phosphorous (Ni-P) alloy coatings were developed on mild steel from a citrate bath using glycerol as an additive. Multilayer Ni-P alloy coatings having nanolaminated layers of alloys of alternatively different compositions have been developed using pulsed direct current (DC) by cyclic modulation of the cathode current density. The composition and number (hence thickness) of the layers were tailored by periodic modulation of the current density (c.d.) and time using a programmable power source. The deposition conditions were optimized for both the composition and thickness of the individual layers for the best performance of the coatings against corrosion. Electrochemical corrosion study, evaluated by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) demonstrated that the multilayer Ni-P alloy coating with 300 nanolaminated layers, represented as (Ni-P)1.0/4.0/300 showed several fold better corrosion resistance compared to its monolayer counterpart (deposited using regular DC) from the same electrolytic bath. Drastic improvement in the corrosion protection efficacy of the nanolaminated multilayer Ni-P alloy coatings were attributed to an increase in number of interfaces, separating layers of alloys having different morphologies, compositions and phase structures, which was supported by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD) analyses, respectively. The corrosion rates of the multilayer Ni-P alloy coatings were decreased with increasing number of layers, only up to an optimal level and then increased. The increase in corrosion rates at a higher degree of layering were attributed to the diffusion of layers, due to the very short deposition time of each layer. © The Royal Society of Chemistry 2016.
Effect of current density during electrodeposition on microstructure and hardness of textured Cu coating in the application of antimicrobial Al touch surface
(Elsevier Ltd, 2016) Augustin, A.; Huilgol, P.; Udupa, K.R.; Bhat, K.U.
Copper is a well proven antimicrobial material which can be used in the form of a coating on the touch surfaces. Those coating can offer a good service as touch surface for very long time if only they possess good mechanical properties like scratch resistance and microhardness. In the present work the above mentioned mechanical properties were determined on the electrodeposited copper thin film; deposited on double zincated aluminium. During deposition, current density was varied from 2 A dm?2 to 10 A dm?2, to produce crystallite size in the range of 33.5 nm to 66 nm. The crystallite size was calculated from the X-ray peak broadening (Scherrer?s formula) which were later confirmed by TEM micrographs. The scratch hardness and microhardness of the coating were measured and correlated with the crystallite size in the copper coating. Both characteristic values were found to increase with the reduction in crystallite size. Reduced crystallite size (Hall–Petch effect) and preferred growth of copper films along (111) plane play a significant role on the increase in the hardness of the coating. Further, TEM analysis reveals the presence of nano-twins in the film deposited at higher current density, which contributed to a large extent to the sharp increase of coating hardness compared to the mechanism of Hall–Petch effect. The antimicrobial ability of the coated sample has been evaluated against Escherichia coli bacteria and which is compared with that of commercially available bulk copper using the colony count method. 94% of E. coli cells were died after six hours of exposure to the copper coated surface. The morphology of the copper treated cells was studied using SEM. © 2016 Elsevier Ltd
Effect of equal channel angular pressing on the microstructure and mechanical properties of Al-10Zn-2Mg alloy
(2018) Manjunath, G.K.; Kumar, G.V.P.; Bhat, K.U.
The current investigation is focused on evaluating the mechanical properties and the microstructure of cast Al-10Zn-2Mg alloy processed through equal channel angular pressing (ECAP). The ECAP processing was attempted at minimum possible processing temperature. Microstructural characterization was carried out in optical microscopy, scanning electron microscopy, transmission electron microscopy and X-ray diffraction analysis. Hardness measurement and tensile tests were employed to estimate the mechanical properties. Experimental results showed that, ECAP processing leads to noticeable grain refinement in the alloy. Reasonable amount of dislocations were observed in the ECAP processed material. After ECAP processing, precipitates nucleation in the material was detected in the XRD analysis. ECAP leads to considerable enhancement in the mechanical properties of the material. After ECAP processing, microhardness of the material is increased from 144 Hv to 216 Hv. Also, after ECAP processing the UTS of the material is increased from 140 MPa to 302 MPa. The increase in the mechanical properties of the alloy after ECAP processing is due to the dislocation strengthening and grain refinement strengthening. Finally, fracture surface morphology of the tensile test samples also studied. � 2018 Author(s).
Effect of equal channel angular pressing on the microstructure and mechanical properties of Al-10Zn-2Mg alloy
(American Institute of Physics Inc. subs@aip.org, 2018) Manjunath, G.K.; Preetham Kumar, G.V.; Bhat, K.U.
The current investigation is focused on evaluating the mechanical properties and the microstructure of cast Al-10Zn-2Mg alloy processed through equal channel angular pressing (ECAP). The ECAP processing was attempted at minimum possible processing temperature. Microstructural characterization was carried out in optical microscopy, scanning electron microscopy, transmission electron microscopy and X-ray diffraction analysis. Hardness measurement and tensile tests were employed to estimate the mechanical properties. Experimental results showed that, ECAP processing leads to noticeable grain refinement in the alloy. Reasonable amount of dislocations were observed in the ECAP processed material. After ECAP processing, precipitates nucleation in the material was detected in the XRD analysis. ECAP leads to considerable enhancement in the mechanical properties of the material. After ECAP processing, microhardness of the material is increased from 144 Hv to 216 Hv. Also, after ECAP processing the UTS of the material is increased from 140 MPa to 302 MPa. The increase in the mechanical properties of the alloy after ECAP processing is due to the dislocation strengthening and grain refinement strengthening. Finally, fracture surface morphology of the tensile test samples also studied. Â© 2018 Author(s).
Effect of filler wire strength on high strength low alloy steels
(Elsevier Ltd, 2021) John, M.; Kumar, P.A.; Bhat, K.U.
Fusion welding of Ti-Nb microalloyed steels often leads to softening in the heat affected zone (HAZ) due to weld thermal cycles. Apart from heat input and width of HAZ, selection of filler wire also plays an important role, to achieve the minimum strength requirement of the parent material. Steel plates with 800 MPa ultimate tensile strength were butt welded using pulsed gas metal arc welding (P-GMAW) process, with undermatching, matching and overmatching strength filler wires. Welding parameters were selected in such a way that the heat input per unit weld length is almost constant. In all the samples, microstructural features were similar in the HAZ region. Static tensile tests indicated that failure in the samples welded using undermatching filler occurred at welded region, whereas the samples welded with matching and overmatching fillers failed at HAZ region. Further fracture studies indicated that, in case of under matching filler wire samples, crack propagates along the Widmanstatten ferrite present in the weld zone, whereas in other two samples, crack initiated at coarse TiN - matrix interface in the HAZ region. This study shows that overmatching fillers are recommended to overcome strength loss due to HAZ softening. Â© 2021 Elsevier Ltd. All rights reserved. Selection and Peer-review under responsibility of the scientific committee of the Global Conference on Recent Advances in Sustainable Materials 2021.
Effect of nickel sulphate to hypophosphite ratio on the electroless deposition of Ni-P coatings on aluminium
(Trans Tech Publications, 2014) Jayalakshmi, M.; Bhat, K.U.
Electroless Ni-P alloy was deposited on commercial pure aluminium with different nickel source-reducing species ratios. Deposition time was fixed as two hours. The deposits were characterised for changes in morphology and crystallinity. It was observed that increase in nickel source to reducing species ratio produced a deposit with reduced mean nodule size. Also, nodule size distribution was narrow. Deposits with increased ratio showed higher levels of crystallinity. Â© (2014) Trans Tech Publications, Switzerland.
Effect of retrogression duration on the grain boundary microstructure and microchemistry of AA7010
(2018) Nandana, M.S.; Bhat, K.U.; Manjunatha, C.M.
The paper presents the microstructural characterization of the aluminium alloy 7010 in retrogression and re- ageing (RRA) condition by using Transmission Electron Microscope (TEM). The grain boundary microstructure is analyzed with the focus on variation of GBP's (grain boundary precipitate) size and PFZ (precipitate free zone) size during retrogression performed at 200 �C for duration of 10-60 min. The microchemistry of the GBP's is analyzed by using TEM-EDS (Energy Dispersive X-ray spectroscopy). The results reveal the coarsening of discrete GBP's along with enrichment of the Cu in them. The average size of the GBP's in RRA treated sample vary from 30 nm during 10 min of retrogression to 59 nm at 60 min of retrogression. The PFZ size varied from 35 nm to 51 nm for 10 min and 60 min of retrogression time, respectively. The Cu content of the GBP's increased from 3.54 wt% for 10 min of retrogression to 5.27 wt% for 60 min of retrogression and re-aged sample. � 2018 Author(s).
Effect of retrogression duration on the grain boundary microstructure and microchemistry of AA7010
(American Institute of Physics Inc. subs@aip.org, 2018) Nandana, M.S.; Bhat, K.U.; Manjunatha, C.M.
The paper presents the microstructural characterization of the aluminium alloy 7010 in retrogression and re- ageing (RRA) condition by using Transmission Electron Microscope (TEM). The grain boundary microstructure is analyzed with the focus on variation of GBP's (grain boundary precipitate) size and PFZ (precipitate free zone) size during retrogression performed at 200 Â°C for duration of 10-60 min. The microchemistry of the GBP's is analyzed by using TEM-EDS (Energy Dispersive X-ray spectroscopy). The results reveal the coarsening of discrete GBP's along with enrichment of the Cu in them. The average size of the GBP's in RRA treated sample vary from 30 nm during 10 min of retrogression to 59 nm at 60 min of retrogression. The PFZ size varied from 35 nm to 51 nm for 10 min and 60 min of retrogression time, respectively. The Cu content of the GBP's increased from 3.54 wt% for 10 min of retrogression to 5.27 wt% for 60 min of retrogression and re-aged sample. Â© 2018 Author(s).
Effect of shot peening coverage on surface nanostructuring of 316L stainless steel and its influence on low temperature plasma-nitriding
(ASTM International, 2017) Jayalakshmi, M.; Badekai Ramachandra, B.; Bhat, K.U.
Air-blast shot peening (ABSP) is a cost effective and industrially viable technique to produce nanostructured surface layer on metallic materials. In the present study, 316L stainless steel samples were subjected to shot peening at different peening coverage, from conventional to severe peening. Nanocrystalline structure was observed on the sample surface after peening and mechanical twins; intersection of multidirectional twins producing rhombic blocks were observed in the subsurface layer. Peening process led to the formation of strain induced martensite (?'), and its fraction was found to increase with the coverage. Depth of nanostructured layer and surface microhardness also increased with the increase in coverage, whereas surface roughness followed an opposite trend. Both peened and un-peened samples were subjected to plasma nitriding at 400°C for 4 h. Uniform and appreciably high case depth of about 45 ?m was observed in severely pre-peened (1000 % coverage) sample after nitriding treatment. No precipitation of CrN was observed. This highlights the marked influence of severe shot peening as a pre-treatment for low temperature plasma nitriding of austenitic stainless steels. © © 2017 by ASTM International.
Effect of solvent on the morphology of MoS2 nanosheets prepared by ultrasonication-assisted exfoliation
(2018) Prabukumar, C.; Sadiq, M.M.J.; Bhat, D.K.; Bhat, K.U.
The MoS2 nanosheets are prepared via liquid-phase exfoliation route. Bulk MoS2 powder is exfoliated by ultrasonication-assisted method with the aid of different solvents. The effect of solvents used on the morphology of the MoS2 nanosheets is investigated. The exfoliated material is analysed by using scanning electron microscopy, transmission electron microscopy, Fourier-transform infrared spectroscopy and X-ray diffractometry. The MoS2 nanosheets exfoliated by using NMP-water mixture showed the better morphology than that exfoliated with the other solvent mixtures. � 2018 Author(s).
Effect of solvent on the morphology of MoS2 nanosheets prepared by ultrasonication-assisted exfoliation
(American Institute of Physics Inc. subs@aip.org, 2018) Prabukumar, C.; Mohamed, M.M.J.; Bhat, D.K.; Bhat, K.U.
The MoS2 nanosheets are prepared via liquid-phase exfoliation route. Bulk MoS2 powder is exfoliated by ultrasonication-assisted method with the aid of different solvents. The effect of solvents used on the morphology of the MoS2 nanosheets is investigated. The exfoliated material is analysed by using scanning electron microscopy, transmission electron microscopy, Fourier-transform infrared spectroscopy and X-ray diffractometry. The MoS2 nanosheets exfoliated by using NMP-water mixture showed the better morphology than that exfoliated with the other solvent mixtures. Â© 2018 Author(s).